Solution-combustion synthesis of oxide nanoparticles from nitrate solutions containing glycine and urea: Thermodynamic aspects

被引：21
|
作者：
Khaliullin S.M. [1 ]
Zhuravlev V.D. [1 ]
Bamburov V.G. [1 ]
机构：
[1] Institute of Solid State Chemistry, Ural Branch, Russian Academy of Sciences, ul. Pervomaiskaya 91, Yekaterinburg
来源：
International Journal of Self-Propagating High-Temperature Synthesis | 2016年 / 25卷 / 3期
关键词：
adiabatic reaction; glycine; ionic radius; metal oxides; solution-combustion synthesis (SCS); temperature effect; urea;
D O I：
10.3103/S1061386216030031
中图分类号：
学科分类号：
摘要：
Solution-combustion synthesis (SCS) of nanoparticles was characterized by the temperature effect (ΔTad) calculated upon neglect by the temperature dependence of heat capacity. Thus calculated ΔTad values were found to be a linear function of the inverse radius of metal ions. Our calculations have shown that SCS reactions may yield not only oxides but also hydroxides and carbonates. Suggested was a simple formula for evaluating the ΔTad values attained in SCS of complex oxides. © 2016, Allerton Press, Inc.
引用
收藏
页码：139 / 148
页数：9
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