Optimized and validated wavelength-dispersive X-ray fluorescence spectrometry (WDXRF) method for the determination of uranium in phosphogypsum

被引:0
|
作者
Mohamed Guitouni
机构
[1] National Institute of Research and Physico-Chemical Analysis,X
关键词
X-ray fluorescence analysis; Natural uranium; Uranium phosphates; Chemical effluents; Radioactives effluents;
D O I
暂无
中图分类号
学科分类号
摘要
An optimized and validated wavelength-dispersive X-ray fluorescence spectrometry method has been developed for the determination of uranium in phosphogypsum. The method is based on the measurement of the intensities of the Lα1 line for uranium. The concentration of uranium in the phosphogypsum is in the order of 100 ppm with a coefficient of variation of 0.7 %. The method was validated in the concentration range of (0–125) ppm and the different criteria: linearity, specificity, accuracy, repeatability and reproducibility were tested and found acceptable.
引用
收藏
页码:1649 / 1657
页数:8
相关论文
共 50 条
  • [41] Determination of water content in silica nanopowder using wavelength-dispersive X-ray fluorescence spectrometer
    Choi, Yong Suk
    Kim, Jong-Yun
    Yoon, Suk Bon
    Song, Kyuseok
    Kim, Young Jin
    MICROCHEMICAL JOURNAL, 2011, 99 (02) : 332 - 338
  • [42] A knowledge-controlled method for sequential wavelength-dispersive X-ray spectrometry: a feasibility study
    Dane, AD
    Janssen, FEDOR
    vanSprang, HA
    Bekkers, M
    Buydens, LMC
    ANALYTICA CHIMICA ACTA, 1997, 351 (1-3) : 359 - 375
  • [43] Determination of Chlorides in Ionic Liquids by Wavelength Dispersive X-ray Fluorescence Spectrometry
    Vereycken, Willem
    Riano, Sofia
    Van Gerven, Tom
    Binnemans, Koen
    ACS OMEGA, 2021, 6 (21): : 13620 - 13625
  • [44] Absolute Determination of Characteristic X-Ray Yields with a Wavelength-Dispersive Spectrometer
    Claude Merlet
    Xavier Llovet
    Microchimica Acta, 2006, 155 : 199 - 204
  • [45] Comparison of wavelength-dispersive X-ray fluorescence spectrometry and inductively coupled plasma optical emission spectrometry for the elementary determination in plants through the accuracy profile method
    Masson, Pierre
    Dalix, Thierry
    Daugey, Guillaume
    Soule, Patrice
    X-RAY SPECTROMETRY, 2018, 47 (04) : 287 - 293
  • [46] Advances in analysis of low-atomic-number elements by wavelength-dispersive x-ray fluorescence spectrometry
    Vrebos, B
    SPECTROSCOPY, 1997, 12 (06) : 54 - 58
  • [47] Absolute determination of characteristic x-ray yields with a wavelength-dispersive spectrometer
    Merlet, Claude
    Llovet, Xavier
    MICROCHIMICA ACTA, 2006, 155 (1-2) : 199 - 204
  • [48] COMPUTER METHOD FOR QUALITATIVE WAVELENGTH-DISPERSIVE X-RAY-FLUORESCENCE ANALYSIS
    VILA, E
    BERMUDEZPOLONIO, J
    JIMENEZSECO, JL
    X-RAY SPECTROMETRY, 1984, 13 (04) : 187 - 191
  • [49] Determination of chemical composition of siderite in concretions by wavelength-dispersive X-ray spectrometry following selective dissolution
    Sitko, Rafal
    Zawisza, Beata
    Krzykawski, Tomasz
    Malicka, Ewa
    TALANTA, 2009, 77 (03) : 1105 - 1110
  • [50] Analysis of Micronutrients and Heavy Metals in Portuguese Infant Milk Powders by Wavelength Dispersive X-ray Fluorescence Spectrometry (WDXRF)
    Tânia A. P. Fernandes
    José A. A. Brito
    Luísa M. L. Gonçalves
    Food Analytical Methods, 2015, 8 : 52 - 57