Crystal structure of [CuL](NO3)(ReO4) and [CuL](ReO4)2 (L = 4,6,6-trimethyl-1,9-diamino-3,7-diazanon-3-en)

被引：0
|
作者：
E. A. Bykova
S. P. Khranenko
E. Yu. Semitut
S. A. Gromilov
机构：
[1] Russian Academy of Sciences,A. V. Nikolaev Institute of Inorganic Chemistry, Siberian Division
[2] Novosibirsk State University,Research and Education Complex “Nanosystems and Modern Materials,”
来源：
Journal of Structural Chemistry | 2012年 / 53卷
关键词：
copper; rhenium; crystal chemistry; single crystal X-ray diffraction; thermal studies;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
The crystal structures of [CuL](NO3)(ReO4) and [CuL](ReO4)2 (L is 4,6,6-trimethyl-1,9-diamino-3,7-diazanon-3-en) are studied. The square coordination of the copper atom in [CuL](NO3)(ReO4) is completed to a distorted octahedron by two oxygen atoms: Cu…O (ReO4−) 2.393 Å and Cu…O (NO3−) 2.685 Å, and that in [CuL](ReO4)2, by Cu…O(ReO4−) 2.468 Å and 2.697 Å. The products of thermolysis of the salts in a hydrogen atmosphere at 800°C are mixtures of nanocrystalline metal powders with coherent scattering regions of ∼45 nm.
引用
收藏
页码：138 / 144
页数：6
相关论文
共 50 条
  • [21] Rhenium(V) complexes with benzimidazole (BzimH) and crystal structure of the hemiprotonated compound [ReO2(BzimH)(4)][ReO(OH)(BzimH)(4)](ReO4)(3)
    Belanger, S
    Fortin, S
    Beauchamp, AL
    CANADIAN JOURNAL OF CHEMISTRY-REVUE CANADIENNE DE CHIMIE, 1997, 75 (01): : 37 - 45
  • [22] Comparison of vibrational dynamics, thermal behaviour, and phase transition in [Ni(NH3)4](ReO4)2 and [Ni(NH3)6](ReO4)2
    Hetmanczyk, Lukasz
    Hetmanczyk, Joanna
    JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY, 2015, 119 (02) : 1415 - 1428
  • [23] Synthesis and crystal structure of Eu(ReO4)3(H2O)3 and Eu3ReO8
    Mujica, C
    Llanos, J
    Peters, K
    Peters, EM
    von Schnering, HG
    JOURNAL OF ALLOYS AND COMPOUNDS, 1999, 288 (1-2) : 120 - 123
  • [24] Crystal structure and thermal stability of Sm(ReO4)3(H2O)3
    Mujica, C
    Llanos, J
    Sánchez, V
    Schnelle, W
    Cardoso-Gil, R
    JOURNAL OF ALLOYS AND COMPOUNDS, 2004, 364 (1-2) : 89 - 92
  • [25] Crystal structures of Cd(ReO4)2•4 urea, Cd(ReO4)2•6 urea and Ca(ReO4)2•5 urea.: Synthesis and characterization of urea adducts from the systems M(ReO4)2-urea-H2O, M = Ca, Sr, Ba, Ph and Cd
    Petrova, R
    Todorov, T
    Bakardjieva, S
    Mihailova, B
    Angelova, O
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE, 2000, 215 (05): : 309 - 316
  • [26] Synthesis and crystal structure of the monoclinic modification of Yb(ReO4)3(H2O)4
    Mujica, C
    Llanos, J
    Sánchez, V
    Gómez-Romero, P
    Casañ-Pastor, N
    JOURNAL OF SOLID STATE CHEMISTRY, 2003, 172 (01) : 200 - 204
  • [27] X-ray study of [Cu(NH3)4](ReO4)2-[Cu(NH3)2(μ-ReO4)2] n transformation
    Gromilov, S. A.
    Tyutyunnik, A. P.
    Piryazev, D. A.
    Plyusnin, P. E.
    Korenev, S. V.
    JOURNAL OF STRUCTURAL CHEMISTRY, 2016, 57 (01) : 140 - 145
  • [28] CRYSTAL-STRUCTURE OF ALPHA-(BEDT-TTF)3(REO4)2
    KANBARA, H
    TAJIMA, H
    ARATANI, S
    YAKUSHI, K
    KURODA, H
    SAITO, G
    KAWAMOTO, A
    TANAKA, J
    CHEMISTRY LETTERS, 1986, (03) : 437 - 440
  • [29] Crystal structure of hydroxonitrosotetrammineruthenium(IV) perrhenate [Ru(NO)(OH)(NH3)4](ReO4)2
    Minacheva, LK
    Kokunova, VN
    Sergienko, VS
    Kokunov, YV
    RUSSIAN JOURNAL OF INORGANIC CHEMISTRY, 2001, 46 (08) : 1160 - 1163
  • [30] SYNTHESIS AND CRYSTAL-STRUCTURE OF [RE(2,2'-BIPYRIDINE)3](REO4)2
    STEBLER, M
    GUTIERREZ, A
    LUDI, A
    BURGI, HB
    INORGANIC CHEMISTRY, 1987, 26 (09) : 1449 - 1451
12345