Development of a method for des-glaucine production in a subcritical water medium

被引：0
|
作者：
S. N. Borisenko
A. V. Bicherov
O. V. Pavlyuk
M. I. Rudnev
N. I. Borisenko
E. V. Vetrova
V. I. Minkin
R. N. Borisenko
A. V. Lekar
机构：
[1] Southern Federal University,Institute of Physical and Organic Chemistry
[2] Russian Academy of Sciences,Southern Scientific Center
[3] Environmental Analytical Center of Southern Federal University,undefined
来源：
Russian Journal of Physical Chemistry B | 2009年 / 3卷
关键词：
subcritical water; glaucine; des-glaucine; NMR; ESI MS;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
The isomerization of a non-racemic mixture of glaucine isomers to des-glaucine (seco-glaucine) in a subcritical water medium at 200–300°C was conducted with a yield of 53%. The structure of the product was confirmed by NMR spectroscopy and electrospray-ionization mass spectrometry.
引用
收藏
页码：1131 / 1133
页数：2
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