Products of the interaction of veratrole and paraform in a subcritical water medium

被引：0
|
作者：
S. N. Borisenko
M. I. Rudnev
A. V. Bicherov
O. V. Ryabtsova
N. I. Borisenko
E. V. Vetrova
V. I. Minkin
A. V. Lekar’
机构：
[1] Southern Federal University,Institute of Physical and Organic Chemistry
[2] Russian Academy of Sciences,Southern Scientific Center
[3] Ecological Analytical Center of Southern Federal University,undefined
来源：
Russian Journal of Physical Chemistry B | 2009年 / 3卷
关键词：
subcritical water; veratrole; paraform; cyclotriveratrylene; cyclotetraveratrylene; ESI mass spectrometry; NMR;
D O I：
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学科分类号：
摘要：
The interaction of veratrole and paraform in a subcritical water medium was studied and the macrocyclic compounds (cyclotriveratrylene and cyclotetraveratrylene) were obtained in a ratio of 94: 6. The formation of the aforementioned compounds is confirmed by complex analytical methods, including mass spectrometry with electrospray ionization (ESI MS) and NMR spectroscopy. The data of ESI MS showed that the mixed adducts of the above macrocycles of trimer-cation-tetramer type are formed.
引用
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页码：1113 / 1116
页数：3
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