Structural and magnetic properties of FeCr2S4 spinel prepared by field-activated sintering and conventional solid-state synthesis

被引:0
|
作者
V. Zestrea
V. Y. Kodash
V. Felea
P. Petrenco
D. V. Quach
Joanna R. Groza
Vladimir Tsurkan
机构
[1] University of California,Department of Chemical Engineering and Materials Science
[2] Academy of Science of Moldova,Institute of Applied Physics
来源
关键词
Magnetic Anomaly; Spark Plasma Sinter; Rietveld Refinement; Fast Sample; Cr2S3;
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学科分类号
摘要
We report on the fast preparation of the ternary magnetic semiconductor spinel FeCr2S4 using the Field-Activated Sintering Technique (FAST). The structural (X-ray) and magnetic (Squid) characterization demonstrates a similarity of the properties of the FAST crystals and those prepared by conventional solid-state synthesis. Residual structural disorder in FAST samples has a pronounced influence on the ferrimagnetic–paramagnetic transition and the orbital ordering at low temperatures.
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页码:660 / 664
页数:4
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