Analysis of High-Purity Volatile Compounds

被引:0
|
作者
V. A. Krylov
机构
[1] Institute of High-Purity Substances,
[2] Russian Academy of Sciences,undefined
[3] Nizhni Novgorod State University,undefined
来源
关键词
Analytical Chemistry; Detection Limit; Light Scattering; Organic Substance; Volatile Compound;
D O I
暂无
中图分类号
学科分类号
摘要
The current status of the analysis of high-purity volatile substances is considered. Two types of impurities in high-purity volatile substances were distinguished: molecularly dissolved substances and suspended particles. The main factors that restrict the limiting capabilities of analytical techniques were revealed. The attained detection limits were 10–8–10–10% for metal impurities, 10–4–10–8% for organic substances, 10–5–10–9% for water, and 10–5–10–7 for permanent gases. Suspended particles of 0.04–0.003 μm in size were determined by light scattering.
引用
收藏
页码:660 / 671
页数:11
相关论文
共 50 条
  • [21] PRACTICAL ANALYSIS OF HIGH-PURITY CHEMICALS .6. EMISSION SPECTROGRAPHIC ANALYSIS OF HIGH-PURITY ACIDS
    KERSHNER, NA
    JOY, EF
    BARNARD, AJ
    [J]. APPLIED SPECTROSCOPY, 1971, 25 (05) : 542 - &
  • [22] ATOMIC-ABSORPTION AND EMISSION SPECTROPHOTOMETRY IN ANALYSIS OF HIGH-PURITY MATERIALS - ANALYSIS OF HIGH-PURITY RHENIUM
    ZELENTSOVA, LV
    YUDELEVICH, IG
    SHABUROVA, VP
    [J]. JOURNAL OF ANALYTICAL CHEMISTRY OF THE USSR, 1977, 32 (06): : 918 - 921
  • [23] Development of certified reference materials of high-purity volatile organic compounds: purity assay by the freezing-point depression method
    Yoshitaka Shimizu
    Yoko Ohte
    Xinnu Bao
    Satoko Otsuka
    Yuko Kitamaki
    Keiichiro Ishikawa
    Toshihide Ihara
    Kenji Kato
    [J]. Accreditation and Quality Assurance, 2008, 13 : 389 - 396
  • [24] Gas Chromatography-Mass Spectrometry Analysis of High-Purity Volatile Inorganic Hydrides
    Sozin, A. Yu
    Krylov, V. A.
    Chernova, O. Yu
    Sorochkina, T. G.
    Kotkov, A. P.
    Grishnova, N. D.
    Skosyrev, A., I
    Pushkarev, G., V
    [J]. JOURNAL OF ANALYTICAL CHEMISTRY, 2021, 76 (05) : 535 - 545
  • [25] Development of certified reference materials of high-purity volatile organic compounds: purity assay by the freezing-point depression method
    Shimizu, Yoshitaka
    Ohte, Yoko
    Bao, Xinnu
    Otsuka, Satoko
    Kitamaki, Yuko
    Ishikawa, Keiichiro
    Ihara, Toshihide
    Kato, Kenji
    [J]. ACCREDITATION AND QUALITY ASSURANCE, 2008, 13 (07) : 389 - 396
  • [26] Elemental Impurity Composition of High-Purity Volatile Hydrides and Chlorides
    Lazukina, O. P.
    Malyshev, K. K.
    Volkova, E. N.
    Churbanov, M. F.
    [J]. INORGANIC MATERIALS, 2018, 54 (02) : 176 - 186
  • [27] Elemental Impurity Composition of High-Purity Volatile Hydrides and Chlorides
    O. P. Lazukina
    K. K. Malyshev
    E. N. Volkova
    M. F. Churbanov
    [J]. Inorganic Materials, 2018, 54 : 176 - 186
  • [28] PREPARATION OF HIGH-PURITY VOLATILE ACIDS AND BASES BY ISOTHERMAL DISTILLATION
    VEILLON, C
    REAMER, DC
    [J]. ANALYTICAL CHEMISTRY, 1981, 53 (03) : 549 - 550
  • [29] Preconcentration in the Analysis of High-Purity Volatiles
    V. A. Krylov
    [J]. Journal of Analytical Chemistry, 2003, 58 (7) : 663 - 663
  • [30] SPECTRAL ANALYSIS OF HIGH-PURITY SILICON
    ZILBERSHTEIN, KI
    PIRYUTKO, MM
    EVTUSHENKO, TP
    SAKHARNOVA, IL
    NIKITINA, ON
    [J]. INDUSTRIAL LABORATORY, 1959, 25 (12): : 1547 - 1549