Synthesis and thermal study of new N-substituted 1H-pyrrolo[3,4-c]pyridine-1,3(2H)diones of Mannich base type

被引：0
|
作者：
Edward Krzyżak
Berenika Szczęśniak-Sięga
Dominika Szkatuła
Wiesław Malinka
机构：
[1] Wrocław Medical University,Department of Inorganic Chemistry
[2] Wrocław Medical University,Department of Chemistry of Drugs
来源：
Journal of Thermal Analysis and Calorimetry | 2012年 / 108卷
关键词：
DSC; Polymorphism; Pyridinedicarboximide; Thermal stability;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
The new derivatives of 3,4-pyridinedicarboximide were synthesised. Experimental measurements were carried out using 1H NMR spectra, IR spectra, elemental analyses and differential scanning calorimetry. The purpose of this study was to study the thermal stability of these four new compounds and to establish a solid-state polymorphism. Measurements were carried out for samples obtained from ethanol and n-hexane and after a long-time storage.
引用
收藏
页码：1303 / 1309
页数：6
相关论文
共 50 条
  • [21] SYNTHESIS AND BIOLOGICAL ACTIVITY OF NOVEL 6-PHENYL-1H-PYRROLO[3,4-c]PYRIDINE-1,3-DIONE DERIVATIVES
    Wojcicka, Anna
    Becan, Lilianna
    Junka, Adam
    Bartoszewicz, Marzenna
    Secewicz, Anna
    Trynda, Justyna
    Wietrzyk, Joanna
    ACTA POLONIAE PHARMACEUTICA, 2017, 74 (02): : 435 - 443
  • [22] Access and Modulation of Substituted Pyrrolo[3,4-c]pyrazole-4,6-(2H,5H)-diones
    Ejjoummany, Abdelaziz
    Elie, Jonathan
    El Hakmaoui, Ahmed
    Akssira, Mohamed
    Routier, Sylvain
    Buron, Frederic
    MOLECULES, 2023, 28 (15):
  • [23] Synthesis of C-Glycosyl Pyrrolo[3,4-c]carbazole-1,3(2H,6H)-diones as a Scaffold for Check Point Kinase 1 Inhibitors
    Ichikawa, Satoshi
    Tatebayashi, Nana
    Matsuda, Akira
    JOURNAL OF ORGANIC CHEMISTRY, 2013, 78 (23): : 12065 - 12075
  • [24] Copper(I)-catalysed amidation and successive oxidation of benzylic C(sp3)-H bond: synthesis of 1H-pyrrolo[3,4-b]quinoline-1,3(2H)-diones
    Yan, Xiangqian
    Zhang, Zhiguo
    Zhang, Guisheng
    Ma, Nana
    Liu, Qingfeng
    Liu, Tongxin
    Shi, Lei
    TETRAHEDRON, 2016, 72 (29) : 4245 - 4251
  • [25] NEW SYNTHESIS OF 2H-PYRROLO[3,4-C]QUINOLINES
    FRITZ, H
    SCHENK, S
    ANNALEN DER CHEMIE-JUSTUS LIEBIG, 1975, (02): : 255 - 265
  • [26] [inline-graphic not available: see fulltext] Synthesis of pyrrolo[3,4-c]pyridine-1,3-diones (5-azaphthalimides) (microreview)
    Oleg V. Ershov
    Anastasiya I. Ershova
    Chemistry of Heterocyclic Compounds, 2020, 56 : 518 - 520
  • [27] SYNTHESIS AND PROPERTIES OF 4-ALKOXY-2-[2-HYDROXY-3-(4-o,m,p-HA HALOGENOARYL-1-PIPERAZINYL)PROPYL]-6-METHYL-1H-PYRROLO-[3,4-C]PYRIDINE-1,3(2H)-DIONES WITH ANALGESIC AND SEDATIVE ACTIVITIES
    Sladowska, Helena
    Sabiniarz, Aleksandra
    Szkatula, Dominika
    Filipek, Barbara
    Sapa, Jacek
    ACTA POLONIAE PHARMACEUTICA, 2006, 63 (04): : 245 - 254
  • [28] Synthesis and antimicrobial activity of some Mannich bases of benzimidazolyl substituted 1H-isoindole-1,3(2H) diones
    Rajpurohit, S
    Sah, P
    ASIAN JOURNAL OF CHEMISTRY, 2005, 17 (02) : 949 - 954
  • [29] Synthesis of 2-methoxypyridine-3,4-dicarbonitriles and 4-methoxy-2,3-dihydro-1H-pyrrolo[3,4]pyridine-1,3-diones
    O. V. Ershov
    V. N. Maksimova
    M. Yu. Ievlev
    M. Yu. Belikov
    Kh. R. Khayarov
    O. E. Nasakin
    Russian Journal of Organic Chemistry, 2015, 51 : 1668 - 1670
  • [30] Synthesis of 2-methoxypyridine-3,4-dicarbonitriles and 4-methoxy-2,3-dihydro-1H-pyrrolo[3,4]pyridine-1,3-diones
    Ershov, O. V.
    Maksimova, V. N.
    Ievlev, M. Yu.
    Belikov, M. Yu.
    Khayarov, Kh. R.
    Nasakin, O. E.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2015, 51 (11) : 1668 - 1670
12345