Synthesis and thermal study of new N-substituted 1H-pyrrolo[3,4-c]pyridine-1,3(2H)diones of Mannich base type

被引：0

作者：

Edward Krzyżak

Berenika Szczęśniak-Sięga

Dominika Szkatuła

Wiesław Malinka

机构：

[1] Wrocław Medical University,Department of Inorganic Chemistry

[2] Wrocław Medical University,Department of Chemistry of Drugs

来源：

Journal of Thermal Analysis and Calorimetry | 2012年 / 108卷

关键词：

DSC; Polymorphism; Pyridinedicarboximide; Thermal stability;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

The new derivatives of 3,4-pyridinedicarboximide were synthesised. Experimental measurements were carried out using 1H NMR spectra, IR spectra, elemental analyses and differential scanning calorimetry. The purpose of this study was to study the thermal stability of these four new compounds and to establish a solid-state polymorphism. Measurements were carried out for samples obtained from ethanol and n-hexane and after a long-time storage.

引用

页码：1303 / 1309

页数：6

共 50 条

[1] Synthesis and thermal study of new N-substituted 1H-pyrrolo[3,4-c]pyridine-1,3(2H)diones of Mannich base type
Krzyzak, Edward
Szczesniak-Siega, Berenika
Szkatula, Dominika
Malinka, Wieslaw
JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY, 2012, 108 (03) : 1303 - 1309
[2] Synthesis of New 1H-Pyrrolo[3,4-c]pyridine-1,3(2H)-diones
Klyuchko, S., V
Chumachenko, S. A.
Shablykin, O., V
Brovarets, V. S.
RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2021, 91 (03) : 348 - 356
[3] Bioresearch of New 1H-pyrrolo[3,4-c]pyridine-1,3(2H)-diones
Szkatula, Dominika
Krzyzak, Edward
Mogilski, Szczepan
Sapa, Jacek
Filipek, Barbara
Swiatek, Piotr
MOLECULES, 2020, 25 (24):
[4] Synthesis, Cyclooxygenases Inhibition Activities and Interactions with BSA ofN-substituted 1H-pyrrolo[3,4-c]pyridine-1,3(2H)-diones Derivatives
Krzyak, Edward
Szkatula, Dominika
Wiatrak, Benita
Gebarowski, Tomasz
Marciniak, Aleksandra
MOLECULES, 2020, 25 (12):
[5] Pyrrolo[3,4-c]pyridine-1,3(2H)-diones: A Novel Antimycobacterial Class Targeting Mycobacterial Respiration
van der Westhuyzen, Renier
Winks, Susan
Wilson, Colin R.
Boyle, Grant A.
Gessner, Richard K.
de Melo, Candice Soares
Taylor, Dale
de Kock, Carmen
Njoroge, Mathew
Brunschwig, Christel
Lawrence, Nina
Rao, Srinivasa P. S.
Sirgel, Frederick
van Helden, Paul
Seldon, Ronnett
Moosa, Atica
Warner, Digby F.
Arista, Luca
Manjunatha, Ujjini H.
Smith, Paul W.
Street, Leslie J.
Chibale, Kelly
JOURNAL OF MEDICINAL CHEMISTRY, 2015, 58 (23) : 9371 - 9381
[6] SYNTHESIS AND PHARMACOLOGICAL PROPERTIES OF NEW DERIVATIVES OF 4-ALKOXY-6-METHYL-1H-PYRROLO[3,4-c]PYRIDINE-1,3(2H)-DIONES
Sladowska, Helena
Sabiniarz, Aleksandra
Sapa, Jacek
Filipek, Barbara
ACTA POLONIAE PHARMACEUTICA, 2009, 66 (01): : 57 - 63
[7] Antinociceptive, antiedematous, and antiallodynic activity of 1H-pyrrolo[3,4-c]pyridine-1,3(2H)-dione derivatives in experimental models of pain
Dziubina, Anna
Szkatula, Dominika
Gdula-Argasinska, Joanna
Kotanska, Magdalena
Filipek, Barbara
NAUNYN-SCHMIEDEBERGS ARCHIVES OF PHARMACOLOGY, 2020, 393 (05) : 813 - 827
[8] Antinociceptive, antiedematous, and antiallodynic activity of 1H-pyrrolo[3,4-c]pyridine-1,3(2H)-dione derivatives in experimental models of pain
Anna Dziubina
Dominika Szkatuła
Joanna Gdula-Argasińska
Magdalena Kotańska
Barbara Filipek
Naunyn-Schmiedeberg's Archives of Pharmacology, 2020, 393 : 813 - 827
[9] Synthesis of New 1Н-Pyrrolo[3,4-с]pyridine-1,3(2Н)-diones
S. V. Klyuchko
S. A. Chumachenko
O. V. Shablykin
V. S. Brovarets
Russian Journal of General Chemistry, 2021, 91 : 348 - 356
[10] Cu-Catalyzed Decarboxylative Annulation of N-Phenylglycines with Maleimides: Synthesis of 1H-Pyrrolo[3,4-c]quinoline-1,3(2H)-diones
Lv, Kai-Hong
Chen, Li
Zhao, Ke-hua
Yang, Jia-Ming
Yan, Sheng-Jiao
JOURNAL OF ORGANIC CHEMISTRY, 2023, 88 (04): : 2358 - 2366

← 1 2 3 4 5 →