Investigation of the Hot Deformation Behavior in VDM® Alloy 780 by In Situ High-Energy X-Ray Diffraction

被引:0
|
作者
Massimo Fritton
Frank Kümmel
Andreas Kirchmayer
Andreas Stark
Masood Hafez Haghighat
Bodo Gehrmann
Steffen Neumeier
Ralph Gilles
机构
[1] Heinz Maier-Leibnitz Zentrum,Lehrstuhl Für Werkstoffwissenschaften
[2] Technische Universität München,undefined
[3] Friedrich-Alexander-Universität Erlangen-Nürnberg,undefined
[4] Helmholtz-Zentrum Hereon GmbH,undefined
[5] VDM Metals International GmbH,undefined
关键词
D O I
暂无
中图分类号
学科分类号
摘要
Ni-based superalloys are indispensable for applications in demanding environments, such as the heavily stressed rotating discs in the hot sections of modern gas turbines or jet engines. In this paper, the microstructure evolution during hot deformation to mimic the forging process was investigated in the polycrystalline VDM® Alloy 780 viain situ X-ray diffraction at temperatures of 950, 1000, and 1050 °C. For the tested temperatures, the hot forming led to subgrain formation, the built-up of a texture by rotation of the matrix grains into preferred orientations, and dynamic recrystallization. The influence of the deformation was analyzed depending on the direction of the lattice plane normals to the load direction, for the first five γ-reflections in the diffraction pattern. During uniaxial compressive deformation intensity, maxima develop in the loading direction solely for the γ-(220) reflections, while intensity minima develop for the other reflections which correspond to the formation of a <110> fiber texture. In the transverse direction, all γ-reflections except the (220) have an increased intensity at the maximum specimen strain of 20 pct. Directly after the hot forming, three different cooling rates of 10, 100, and 1000 °C/min and their influence on the microstructure were investigated. The fast and medium cooling rates lead to low recrystallized fractions and a largely preserved deformation texture, whereas the low cooling rate leads to a high recrystallized fraction and a slight remaining texture. Additionally, the diffraction data are complemented by electron microscopy measurements.
引用
收藏
页码:2037 / 2051
页数:14
相关论文
共 50 条
  • [41] DIFFRACTION OF A HIGH-ENERGY CHARACTERISTIC X-RAY BY A PERFECT CRYSTAL
    SHORT, MA
    FALLON, MR
    X-RAY SPECTROMETRY, 1990, 19 (01) : 35 - 37
  • [42] Electrochemical Lithiation Cycles of Gold Anodes Observed by In Situ High-Energy X-ray Diffraction
    Bach, Philipp
    Valencia-Jaime, Irais
    Ruett, Uta
    Gutowski, Olof
    Romero, Aldo H.
    Renner, Frank U.
    CHEMISTRY OF MATERIALS, 2016, 28 (09) : 2941 - 2948
  • [43] Investigating the tetragonal/cubic phase transformation using in situ high-energy x-ray diffraction
    Hoai Nguyen
    Li, Tao
    Chen, Zonghai
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2019, 258
  • [44] INVESTIGATION OF DEFORMATION BEHAVIOR OF INDIVIDUAL PHASES IN COMPOSITES BY X-RAY DIFFRACTION
    CHESKIS, HP
    HECKEL, RW
    JOURNAL OF METALS, 1968, 20 (01): : A113 - &
  • [45] Investigation of Deformation Behavior of Thiourethane Elastomers Using In Situ X-ray Scattering, Diffraction, and Absorption Methods
    Rahmawati, Rahmawati
    Masuda, Shiori
    Cheng, Chao-Hung
    Nagano, Chigusa
    Nozaki, Shuhei
    Kamitani, Kazutaka
    Kojio, Ken
    Takahara, Atsushi
    Shinohara, Naoki
    Mita, Kazuki
    Uchida, Kiminori
    Yamasaki, Satoshi
    MACROMOLECULES, 2019, 52 (18) : 6825 - 6833
  • [46] Structural study of semiconductive CdTe-ZnTe alloy by high-energy X-ray diffraction
    Yoneda, Y
    Matsumoto, N
    Suzuya, K
    Kohara, S
    Mizuki, J
    FERROELECTRICS, 2002, 268 : 277 - 282
  • [47] High temperature micro-deformation behavior of continuous TiNb fiber reinforced TiAl matrix composite investigated by in-situ high-energy X-ray diffraction
    Li, Jinguang
    Hu, Rui
    Zhou, Mi
    Gao, Zitong
    Wu, Yulun
    Luo, Xian
    MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2022, 846
  • [48] In situ X-ray diffraction study of deformation behavior in a Fe/NiTi composite
    Hao, Shijie
    Cui, Lishan
    Shao, Yang
    Jiang, Jiang
    Jiang, Daqiang
    Wang, Shan
    Du, Minshu
    Wang, Yandong
    Brown, Dennis E.
    Ren, Yang
    APPLIED PHYSICS LETTERS, 2012, 101 (22)
  • [49] In situ investigation of α-MnO2 electrocatalyst during electrochemical cycling probed by high-energy synchrotron X-ray diffraction
    Yang, Zhenzhen
    Trahey, Lynn
    Chan, Maria
    Lin, Chikai
    Thackeray, Michael
    Ren, Yang
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2013, 246
  • [50] In-situ high energy X-ray diffraction study of microscopic deformation behavior of martensite variant reorientation in NiTi wire
    Kong, Xiangguang
    Yang, Ying
    Sun, Zhen
    Yang, Hong
    Liu, Yinong
    Ren, Yang
    Cui, Lishan
    Chen, Changfeng
    Hao, Shijie
    APPLIED MATERIALS TODAY, 2021, 22