Fabrication and Pore Size Control of Large-Pore Mesoporous Silica Particles through a Solvent Evaporation Process

被引:0
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作者
Hirobumi Shibata
Taku Ogura
Keishi Nishio
Hideki Sakai
Masahiko Abe
Kazuaki Hashimoto
Mutsuyoshi Matsumoto
机构
[1] Chiba Institute of Technology,Department of Life and Environmental Sciences
[2] Tokyo University of Science,Department of Pure and Applied Chemistry
[3] Tokyo University of Science,Department of Materials Science and Technology
[4] Tokyo University of Science,Research Institute for Science and Technology
来源
Silicon | 2011年 / 3卷
关键词
Mesoporous silica; Solvent evaporation; Supramolecular template; Interplanar spacing;
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摘要
Large-pore mesoporous silica particles were synthesized through a solvent evaporation process using hydrophobic fumed silica particles and tetraethyl orthosilicate (TEOS) as silica sources. The solvent evaporation of an ethanol solution of fumed silica particles, TEOS, HCl and triblock copolymer (F127) resulted in mesoporous silica particles with pores with sizes of about 7 nm. In addition, the interplanar spacing of the mesoporous silica particles can be controlled by changing the solvent evaporation temperatures.
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页码:139 / 143
页数:4
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