Determination of perfume oil in household products by headspace solid-phase microextraction and fast capillary gas chromatography

被引:0
|
作者
F. Bothe
K. Dettmer
W. Engewald
机构
[1] Universität Leipzig,Institut für Analytische Chemie
[2] Institute of Tropospheric Research,Department of Entomology
[3] University of California Davis,undefined
来源
Chromatographia | 2003年 / 57卷
关键词
Gas chromatography; Headspace solid-phase microextraction; Fragrance analysis; Household products;
D O I
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中图分类号
学科分类号
摘要
Headspace solid-phase microextraction (HS-SPME) has been successfully applied to the determination of perfume components in scented candle wax, liquid laundry detergent, and fabric softener. Different fiber coatings (100 μm polydimethylsiloxane, 50/30 μm divinylbenzene/Carboxen/polydimethylsiloxane, 70 μm Carbowax/divinylbenzene, and 85 μm polyacrylate) were tested and the extraction conditions were optimized. For most compounds extraction efficiency, reproducibility, and long-term stability were highest for polydimethylsiloxane.
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页码:S199 / S206
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