Controlled-Potential Coulometric Determination of Ruthenium in Ru(OH)Cl3 with Microwave Sample Preparation

被引：0

作者：

N. A. Ezerskaya

E. S. Toropchenova

D. B. Pachgin

I. N. Kiseleva

机构：

[1] Russian Academy of Sciences,Kurnakov Institute of General and Inorganic Chemistry

来源：

Journal of Analytical Chemistry | 2004年 / 59卷

关键词：

Analytical Chemistry; Microwave; Sample Preparation; Ruthenium; Microwave Irradiation;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

A procedure for the controlled-potential coulometric (CPC) determination of ruthenium is proposed. The procedure is based on the redox reaction [Ru(CO)Cl5]2–/[Ru(CO)Cl4(H2O)]2– followed by the synthesis of the [Ru(CO)Cl5]2– depolarizing complex under microwave irradiation. The procedure was used in the analysis of a domestic commercial Ru(OH)Cl3 preparation.

引用

页码：296 / 299

页数：3

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