Structure analysis of [Be(NCS)2(C5H5N)2]

被引：0
|
作者：
H. Böhland
W. Hanay
M. Noltemeyer
A. Meller
H. G. Schmidt
机构：
[1] Department of Chemistry,
[2] Pädagogische Hochschule Erfurt,undefined
[3] Postfach 307,undefined
[4] D-99006 Erfurt,undefined
[5] Germany,undefined
[6] Institute of Inorganic Chemistry,undefined
[7] Georg-August-University Göttingen,undefined
[8] Tammannstrasse 4,undefined
[9] D-37077 Göttingen,undefined
[10] Germany,undefined
来源：
Fresenius' Journal of Analytical Chemistry | 1998年 / 361卷
关键词：
Hydrogen; Chemical Analysis; Hydrogen Bonding; Pyridine; Structure Analysis;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
[Be(NCS)2(C5H5N)2] was prepared and characterized by chemical analysis, FT-IR-analysis, and single crystal X-ray structure analysis. The crystals are orthorhombic with a = 829.30(10) pm, b = 1292.1(2) pm, c = 1313.40(10) pm, space group Pnma. Z = 4. The structure is built up from tetrahedra. Hydrogen bonding between the S-atom of one Be-N-bonded thiocyanate and 1.3-H-atoms of pyridine ligands yield a three dimensional network consisting of folded sheets.
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页码：725 / 728
页数：3
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