MoO3 − δ nanorods

被引:0
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作者
V. L. Volkov
G. S. Zakharova
M. V. Kuznetsov
机构
[1] Russian Academy of Sciences,Institute of Solid State Chemistry, Ural Division
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关键词
Sodium Molybdate; Molybdenum Trioxide; Molybdic Acid; Chemical Current Source; Nanorod Formation;
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摘要
Oxygen-deficient molybdenum trioxide nanorods of composition MoO2.987 (orthorhombic, a = 3.951(2) Å, b = 13.856(1) Å, c = 3.700(1) Å) were synthesized by a hydrothermal process (150–180°C, 30–50 h). MoO3 − δ particles were 60–90 nm in diameter; their lengths were several micrometers. X-ray photoelectron and IR spectra of these nanorods were studied, The nanorods had weak paramagnetism, signifying the existence of molybdenum(V) ions in their structure.
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页码:1686 / 1690
页数:4
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