Syntheses, Characterization and Crystal Structures of Diorganotin(IV) Selenites: 1D Helical Double-Chain Containing Eight-Membered Sn2O4Se2 Inorganic Ring

被引：0

作者：

Chunlin Ma

Jing Ru

Zhenxing Li

Rufen Zhang

机构：

[1] Liaocheng University,Department of Chemistry

来源：

Journal of Inorganic and Organometallic Polymers and Materials | 2012年 / 22卷

关键词：

Diorganotin(IV) selenite; Areneseleninic acid; X-ray crystallography;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

Three new diorganotin(IV) selenites, [Bu2Sn(O2SeC6H5OMe)2]n (1), [Me2Sn(O2SeC6H4CHMe2)2]n (2), [Me2Sn(O2SeC6H4Et)2]n (3) have been synthesized and structurally characterized by elemental analysis, FT-IR, NMR (1H, 13C and 119Sn) spectra, TGA, and X-ray crystallography. The X-ray reveals that complexes 1–3 are 1D infinite double-chain polymers. The molecular of complex 1 is further linked by intermolecular C–H···O interactions to form a 2D network polymer. Complex 3 is linked by C–H···O interactions to form a 3D organotin framework.

引用

页码：1287 / 1292

页数：5

共 44 条

[41] Synthesis and characterization of tributyltin(IV) complexes of 2-[(E)-2-(3-formyl-4-hydroxyphenyl)-1-diazenyl]benzoic acid and 4-[((E)-1-{2-hydroxy-5-[(E)-2-(2-carboxyphenyl)-1-diazenyl]phenyl}methylidene)amino]aryls -: crystal structures of polymeric (Bu3Sn[O2CC6H4{N=N(C6H3-4-OH-5-CHO)}-o])n and (Bu3Sn[O2CC6H4{N=N(C6H3-4-OH-C(H)=NC6H4Cl-4))}-o])n -: toxicity studies on the second instar of Aedes aegypti mosquito larvae
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JOURNAL OF ORGANOMETALLIC CHEMISTRY, 2004, 689 (25) : 4702 - 4711
[42] Different oxidation states of copper(I, I/II, II) thiocyanate complexes containing 1,2,4-triazole as a bridging ligand:: Syntheses, crystal structures, and magnetic properties of 2-D polymer CuI(admtrz)SCN, linear trinuclear [CuI2CuII(admtrz)6(SCN)2](ClO4)2, and triangular trinuclear [CuII3(admtrz)4(SCN)3(μ3-OH)(H2O)](ClO4)2•H2O(admtrz = 4-amino-3,5-dimethyl-1,2,4-triazole)
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[44] Synthesis, characterization and crystal structures of homo- and hetero-substituents containing trans six-coordinate tin(IV) complexes of H2tmtaa (5,14-dihydro-6,8,15,17-tetramethyldibenzo[b,i] [1,4,8,11]tetraazacyclotetradecine), and the solid state NMR spectra study of 119Sn
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