Facile synthesis of micron-sized thiol-functional polysilsesquioxane microspheres through a one-step sol-gel method

被引：0
|
作者：
Lu Han
Zhenyu Nie
Rongsheng Gao
Chengyou Kan
机构：
[1] Tsinghua University,Department of Chemical Engineering and Key Laboratory of Advanced Materials of Ministry of Education
来源：
Journal of Sol-Gel Science and Technology | 2024年 / 109卷
关键词：
Polysilsesquioxane; Micron-sized microsphere; One-step method; Sol-gel method; Thiol-functionalization;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
Micron-sized TPMs are prepared by a one-step base-catalyzed method in the presence of PVP.Monodisperse small TPMs with a Dmean of about 4 μm are synthesized without stirring by nucleation and growth.Large TPMs with a Dmean larger than 10 μm are formed due to the coalescence of oligomer droplets with stirring.
引用
收藏
页码：330 / 345
页数：15
相关论文
共 50 条
  • [41] Synthesis of Au/Co9S8composite aerogels by one-step sol-gel method as hydrogen evolution reaction electrocatalysts
    Ehsan, Muhammad A.
    Khalafallah, Diab
    Zhi, Mingjia
    Hong, Zhanglian
    [J]. JOURNAL OF POROUS MATERIALS, 2021, 28 (01) : 99 - 108
  • [42] Synthesis of SBA-15 Loaded CeO2 Nanocrystals via Sol-gel One-step Process
    Li Jian-Sheng
    Gu Juan
    Xia Min-Ya
    Yuan Jin-Fang
    Sun Xiu-Yun
    Wang Lian-Jun
    [J]. ACTA CHIMICA SINICA, 2008, 66 (20) : 2305 - 2308
  • [43] One-step synthesis of yttrium orthoferrite nanocrystals via sol-gel auto-combustion and their structural and magnetic characteristics
    Zhang, Wei
    Fang, Caixiang
    Yin, Wenhui
    Zeng, Yanwei
    [J]. MATERIALS CHEMISTRY AND PHYSICS, 2013, 137 (03) : 877 - 883
  • [44] The one-step pyrolysis process of rattan-based silicon carbide multiphase ceramics prepared by sol-gel method
    Li, Shijie
    Cui, Heshuai
    Ma, Qianli
    Liu, Xing'e
    Wang, Youhong
    Shang, Lili
    Zheng, Yu
    [J]. JOURNAL OF WOOD SCIENCE, 2021, 67 (01)
  • [45] PVDF-HFP/silica-SH nanocomposite synthesis for PEMFC membranes through simultaneous one-step sol-gel reaction and reactive extrusion
    Seck, S.
    Magana, S.
    Prebe, A.
    Niepceron, F.
    Bounor-Legare, V.
    Bigarre, J.
    Buvat, P.
    Gerard, J. F.
    [J]. MATERIALS CHEMISTRY AND PHYSICS, 2015, 163 : 54 - 62
  • [46] Structural and magnetic properties of GdFeO3 nanomaterial prepared through one-step sol-gel auto combustion technique
    Savaliya, Payalkumari M.
    Ajudiya, Shyam R.
    Sahoo, Jayaprakash
    Katba, Savan
    Tanna, Ashish R.
    [J]. JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY, 2024, 110 (02) : 434 - 442
  • [47] Enhanced catalytic efficiency of FeMnTiOx SCR catalysts through adding tourmaline nanopowders during the one-step sol-gel process
    Xie, Zhibo
    Wang, Fei
    Liang, Jinsheng
    Wang, Zishuo
    Hui, Na
    Ding, Yan
    [J]. MATERIALS LETTERS, 2018, 217 : 60 - 63
  • [48] Production of Ethylene through Ethanol Dehydration on SBA-15 Catalysts Synthesized by Sol-gel and One-step Hydrothermal Methods
    Autthanit, Chaowat
    Jongsomjit, Bunjerd
    [J]. JOURNAL OF OLEO SCIENCE, 2018, 67 (02) : 235 - 243
  • [49] Size-Controlled Synthesis of Monodispersed Poly(3-mercaptopropylsilsesquioxane) Microspheres by a Two-Step Sol-Gel Method
    Lu, Xin
    Hou, Yuhui
    Zha, Jie
    Xin, Zhong
    [J]. INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH, 2014, 53 (38) : 14659 - 14663
  • [50] Effect of precursor material, pH, and aging on ZnO nanoparticles synthesized by one-step sol-gel method for photodynamic and photocatalytic applications
    Sheikhi, Somayeh
    Aliannezhadi, Maryam
    Tehrani, Fatemeh Shariatmadar
    [J]. EUROPEAN PHYSICAL JOURNAL PLUS, 2021, 137 (01):
12345