Reaction of 6-arylidene-2,2-dimethylcyclohexanones with phenylhydrazine. Molecular and crystal structures of 3-(4-halophenyl)-1-phenyl-4,5,6,7-tetrahydro-(2H)-indazoles

被引：0
|
作者：
M. M. Gar
A. V. Eremeev
K. Yu. Suponitsky
S. V. Popkov
机构：
[1] D. I. Mendeleev University of Chemical Technology of Russia,A. N. Nesmeyanov Institute of Organoelement Compounds
[2] Russian Academy of Sciences,undefined
来源：
Russian Chemical Bulletin | 2014年 / 63卷
关键词：
6-arylidene-2,2-dimethylcyclohexanones; 3-aryl-7,7-dimethyl-2-phenyl-3,3a,4,5,6,7-hexahydroindazoles; 3-aryl-7,7-dimethyl-2-phenyl-4,5,6,7-tetrahydroindazoles; X-ray diffraction study; phenylhydrazine; cyclocondensation;
D O I：
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中图分类号：
学科分类号：
摘要：
The previously unknown 3-(4-chlorophenyl)-7,7-dimethyl-2-phenyl-3,3a,4,5,6,7-hexahydroindazole 6a and (4-halophenyl)-7,7-dimethyl-1-phenyl-4,5,6,7-tetrahydroindazoles 7a,b were synthesized by the reaction of 6-arylidene-2,2-dimethylcyclohexanones with phenylhydrazine in the presence of pyridine. The molecular and crystal structures of compounds 7a,b were determined by X-ray diffraction.
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页码：1142 / 1147
页数：5
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