Molecular and crystal structure of 4-trifluoro-2-[2-(4-fluorophenyl)hydrazine-1-ylidene]-1-(thiophen -2-yl)butane-1,3-dione

被引：0
|
作者：
A. M. Magerramov
R. A. Alieva
V. I. Mardanova
F. M. Chyragov
A. V. Kurbanov
K. A. Potekhin
机构：
[1] Baku State University,
[2] Vladimir State Humanitarian University,undefined
来源：
Journal of Structural Chemistry | 2012年 / 53卷
关键词：
single crystal X-ray diffraction; crystal structure; β-diketone; 4-trifluoro-2-[2-(4-fluorophenyl)hydrazine-1-ylidene]-1-(thiophen-2-yl)butane-1,3-dione;
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摘要：
Single crystal X-ray diffraction is used to determine the crystal and molecular structure of 4-trifluoro-2-[2-(4-fluorophenyl)hydrazine-1-ylidene]-1-(thiophen-2-yl)butane-1,3-dione. Crystallographic data for C14H8F4N2O2S are as follows: a = 8.2723(6) Å, b = 9.3009(7) Å, c = 9.9895(7) Å; α = 79.224(2)°, β = 75.851(2)°, γ = 72.337(2)°. Triclinic crystal system, P-1 space group, dx = 1.622 g/cm3, V = 704.83(9) Å3, μ = 0.286 mm−1, crystal size 0.30×0.20×0.20 mm, R1 = 0.0891, wR2 = 0.1989.
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页码：202 / 205
页数：3
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