Structure of 2-{2-[3-methyl-3-(2,4,6-trimethylphenyl) cyclobutyl]-2-oxoethyl}isoindole-1,3-dione

被引:0
|
作者
Uğur Sari
İbrahim Yilmaz
Kutalmış Güven
Alaaddin Çukurovali
İlhan Aksoy
机构
[1] Kíríkkale University,Department of Computer Technology, Faculty of Education
[2] Fírat University,Department of Chemistry, Faculty of Science and Arts
[3] Kíríkkale University,Department of Physics, Faculty of Science and Arts
来源
关键词
X-ray; -sustituted phthalimides; crystal structure;
D O I
暂无
中图分类号
学科分类号
摘要
2-{2-[3-Methyl-3-(2,4,6-trimethylphenyl)cyclobutyl]-2-oxoethyl}isoindole-1,3-dione (C24 H25NO3) was synthesized, and its crystal structure was determined by X-ray crystallographic techniques. The compound crystallizes in the triclinic space group P-1, with unit cell parameters: a = 14.109(9) Å, b = 14.130(8) Å, c = 12.152(6) Å, α = 105.62(5)°, β = 113.75(4)°, γ = 98.78(5)°, V = 2039.8(19) Å3, Dc= 1.223 g/cm3, and Z = 4. The crystal structure has two crystallographically independent molecules, I and II. These molecules are held together by weak intermolecular C—H···O interactions, forming a continuous chain. The dihedral angles between the N-substituted phthalimide moiety and cyclobutane ring in molecules I and II are 60.37(14) and 68.18(18)°, respectively.
引用
收藏
页码:571 / 575
页数:4
相关论文
共 50 条
  • [21] 2-(3-Chloropropyl)-2,3-dihydro-1H-isoindole-1,3-dione
    Nagaraj, B
    Yathirajan, HS
    Bolte, M
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O928 - O929
  • [22] EXPERIMENTAL PORPHYRIA INDUCED BY 3-[2-(2,4,6-TRIMETHYLPHENYL)-THIOETHYL]-4-METHYLSYDNONE
    STEJSKAL, R
    ITABASHI, M
    STANEK, J
    HRUBAN, Z
    VIRCHOWS ARCHIV B-CELL PATHOLOGY INCLUDING MOLECULAR PATHOLOGY, 1975, 18 (02) : 83 - 100
  • [23] Thermodynamic properties of poly(2-[3-(6-tetralino)-3-methyl-1-cyclobutyl]-2-hydroxy ethyl methacrylate) and poly[2-(3-mesityl-3-methyl-1-cyclobutyl)-2-oxoethyl methacrylate)
    Ilter, Zuelfiye
    Kaya, Ismet
    Ercan, Selami
    JOURNAL OF MACROMOLECULAR SCIENCE PART A-PURE AND APPLIED CHEMISTRY, 2007, 44 (01): : 21 - 29
  • [24] 2-[2-(3-Chlorophenyl)hydrazinylidene]-1,3-diphenylpropane-1,3-dione
    Bustos, Carlos
    Alvarez-Thon, Luis
    Carcamo, Juan-Guillermo
    Ibanez, Andres
    Sanchez, Christian
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O1450 - U1006
  • [25] 2-(4-Chlorophenyl)-2-oxoethyl 3,4-dimethoxybenzoate
    Fun, Hoong-Kun
    Quah, Ching Kheng
    Vijesh, A. M.
    Isloor, A. M.
    Arulmoli, T.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O3351 - U173
  • [26] Crystal structure of 2-(4-chlorophen-yl)-2-oxoethyl 3-bromobenzoate
    Khan, Imtiaz
    Ibrar, Aliya
    Hameed, Shahid
    White, Jonathan M.
    Simpson, Jim
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : 301 - +
  • [27] 2-(4-Chlorophenyl)-2-oxoethyl 3-(trifluoromethyl)benzoate
    Fun, Hoong-Kun
    Loh, Wan-Sin
    Garudachari, B.
    Isloor, Arun M.
    Satyanarayan, M. N.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O1597 - U2093
  • [28] 2-(4-Fluorophenyl)-2-oxoethyl 3-(trifluoromethyl)benzoate
    Fun, Hoong-Kun
    Arshad, Suhana
    Garudachari, B.
    Isloor, A. M.
    Shivananda, Kammasandra N.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2836 - +
  • [29] Synthesis, Characterization, and Quantum Chemical Calculations of 1-[3-Methyl-3-(2,4,6-trimethylphenyl)cyclobutyl]-2-{[4-(aryl/alkyl)-5-(thiophen-2-yl)-4H-1,2,4-triazol-3-yl]sulfanyl}ethanone Derivatives
    Sarac, K.
    Gelisken, V.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2024, 60 (01) : 93 - 100
  • [30] 2-(4-Chlorophenyl)-2-oxoethyl benzoate
    Fun, Hoong-Kun
    Shahani, Tara
    Garudachari, B.
    Isloor, Arun M.
    Satyganarayan, M. N.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O1802 - U1663