Preparation of silver nanoparticles from silver(I) nano-coordination polymer

被引：33
|
作者：
Akhbari, Kamran [1 ]
Morsali, Ali [1 ]
机构：
[1] Tarbiat Modares Univ, Fac Sci, Dept Chem, Tehran, Iran
来源：
INORGANICA CHIMICA ACTA | 2010年 / 363卷 / 07期
关键词：
Nano-coordination polymer; Silver nanoparticle; Sonochemical; Surfactant; Thermal analysis; CRYSTAL-STRUCTURE; METALLIC SILVER; RAPID EXPANSION; SOLID-STATE; COMPLEXES; PRECURSORS; ANIONS; PERCHLORATE; NETWORKS; LIGANDS;
D O I：
10.1016/j.ica.2010.01.026
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Nanorods of two-dimensional organometallic coordination polymer, [Ag(mu(4)-DPOAc)](n) (1) [DPOAc = diphenylacetate], has been synthesized by the reaction of potassium diphenylacetate (DPOAcK) and AgNO3 by sonochemical process. Reaction conditions, such as the concentration of the initial reagents played important roles in the size and growth process of the final product. Silver nanoparticles were synthesized from nanorods of compound 1. These nano-coordination polymer and nanoparticles were characterized by X-ray powder diffraction (XRD) and scanning electron microscopy (SEM). Thermal stability of nano and crystal samples of compound 1 were studied and compared with each other. (C) 2010 Elsevier B.V. All rights reserved.
引用
收藏
页码：1435 / 1440
页数：6
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