Bis(tetraphenylphosphonium) tris(2-thioxo-1,3-dithiole-4,5-dithiolato) stannate(IV) at 293 K

被引:1
|
作者
Wang, Yan-Ling [1 ]
Wang, Yong-Jin
Yao, Jun
Zhao, Xiu-Tai
Wang, Rui-He
机构
[1] China Univ Petr E China, Sch Petr Engn, Dongying 257061, Peoples R China
[2] Qilu Antibiot Pharmaceut Co Ltd, Dept Res & Dev, Jinan 250105, Peoples R China
关键词
D O I
10.1107/S1600536807012469
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, (C24H20P)(2)[Sn(C3S5)(3)], whose structure has been previously reported in the space group P (1) over bar at 120 K [de Assis, Chohan, Howie, Khan, Low, Spencer, Wardell & Wardell (1999), Polyhedron, 18, 3533 - 3544], has been crystallized in the space group C2/c and its structure has been determined at 293 K. The [Sn(C3S5)(3)](2-) anion possesses C(2)symmetry, with the Sn-IV atom and one C = S group lying on the twofold rotation axis. The crystal packing is stabilized by C H (...) S hydrogen bonds.
引用
收藏
页码:M1147 / M1148
页数:2
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