Synthesis and characterization of nano-sized zirconia powder synthesized by single emulsion-assisted direct precipitation

被引：83

作者：

Chandra, Navin ^{[1
]}

Singh, Deepesh Kumar ^{[1
]}

Sharma, Meenakshi ^{[1
]}

Upadhyay, Ravi Kant ^{[1
]}

Amritphale, S. S. ^{[1
]}

Sanghi, S. K. ^{[1
]}

机构：

[1] CSIR, Adv Mat & Proc Res Inst, Bhopal 462064, MP, India

来源：

JOURNAL OF COLLOID AND INTERFACE SCIENCE | 2010年 / 342卷 / 02期

关键词：

t-ZrO2; Phase transformation; Reverse microemulsion; X-ray diffraction (XRD); MICROEMULSION SYSTEM;

D O I：

10.1016/j.jcis.2009.10.065

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

For the first time, single reverse microemulsion-assisted direct precipitation route has been successfully used to synthesize tetragonal zirconia nanoparticles in narrow size range. The synthesized powder was characterized using FT-IR, XRD and HRTEM techniques. The zirconia nanoparticles obtained were spherical in shape and has narrow particle size distribution in the range of 13-31 nm and crystallite size in the range of 13-23 nm. (C) 2009 Elsevier Inc. All rights reserved.

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页码：327 / 332

页数：6

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