Synthesis and characterization of nano-sized zirconia powder synthesized by single emulsion-assisted direct precipitation

被引：83
|
作者：
Chandra, Navin [1 ]
Singh, Deepesh Kumar [1 ]
Sharma, Meenakshi [1 ]
Upadhyay, Ravi Kant [1 ]
Amritphale, S. S. [1 ]
Sanghi, S. K. [1 ]
机构：
[1] CSIR, Adv Mat & Proc Res Inst, Bhopal 462064, MP, India
来源：
JOURNAL OF COLLOID AND INTERFACE SCIENCE | 2010年 / 342卷 / 02期
关键词：
t-ZrO2; Phase transformation; Reverse microemulsion; X-ray diffraction (XRD); MICROEMULSION SYSTEM;
D O I：
10.1016/j.jcis.2009.10.065
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
For the first time, single reverse microemulsion-assisted direct precipitation route has been successfully used to synthesize tetragonal zirconia nanoparticles in narrow size range. The synthesized powder was characterized using FT-IR, XRD and HRTEM techniques. The zirconia nanoparticles obtained were spherical in shape and has narrow particle size distribution in the range of 13-31 nm and crystallite size in the range of 13-23 nm. (C) 2009 Elsevier Inc. All rights reserved.
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页码：327 / 332
页数：6
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