Synthesis and characterization of 9,9-bis(4-hydroxyphenyl and 4-aminophenyl)dibenzofluorenes: Novel fluorene-based monomers

被引：6
|
作者：
Seesukphronrarak, Surasak [1 ]
Kawasaki, Shinichi [2 ]
Kuwata, Shigeki [3 ]
Takata, Toshikazu [4 ,5 ]
机构：
[1] Tokyo Inst Technol, Dept Organ & Polymer Mat, Tokyo 1528552, Japan
[2] Osaka Gas Co Ltd, Adv Mat Business Promot Dept, Osaka 5540051, Japan
[3] Tokyo Inst Technol, Dept Chem Sci & Engn, Tokyo 1528552, Japan
[4] Tokyo Inst Technol, Sch Mat & Chem Technol, Yokohama, Kanagawa 2268503, Japan
[5] Tokyo Inst Technol, RIPST, Yokohama, Kanagawa 2268503, Japan
来源：
JOURNAL OF POLYMER SCIENCE PART A-POLYMER CHEMISTRY | 2019年 / 57卷 / 24期
关键词：
diamine monomer; dibenzofluorene; dihydroxy monomer; fluorene; polyester; polyimide; refractive index; thermal stability; 9,9-DIARYLFLUORENE MOIETY; POLYESTER; BIREFRINGENCE; POLYMERS; ABILITY; MATRIX; CHAINS; ALLOY;
D O I：
10.1002/pola.29540
中图分类号：
O63 [高分子化学（高聚物）];
学科分类号：
070305 ; 080501 ; 081704 ;
摘要：
Two novel 9,9-difunctionalized fluorene-type monomers, 9,9-bis(4-hydroxyphenyl- and 4-aminophenyl)-2,3:6,7-dibenzofluorenes, are synthesized by the reaction of dibenzenzofluorenone with phenol and aniline. These monomers are used for the preparation of polyester and polyimide as the typical polymers to evaluate the property change such as thermal stability caused by the benzene rings fused to the fluorene skeleton with keeping good solubility, in comparison with the polymers derived from simple fluorenone. In fact, these two new polymers have the fairly enhanced thermal stability and refractive index value along with satisfactory solubility in organic solvents, enough to emphasize the fusion effect. (c) 2019 Wiley Periodicals, Inc. J. Polym. Sci., Part A: Polym. Chem. 2019
引用
收藏
页码：2602 / 2605
页数：4
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