Hydrothermal preparation and characterization of brookite-type TiO2 nanocrystallites

被引:8
|
作者
Zheng, YQ [1 ]
Erwei, S [1 ]
Cui, SX [1 ]
Li, WJ [1 ]
Hu, XF [1 ]
机构
[1] Chinese Acad Sci, Shanghai Inst Ceram, Shanghai 201800, Peoples R China
基金
中国国家自然科学基金;
关键词
D O I
10.1023/a:1011010306699
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Titanium dioxide in brookite form was prepared by two different methods under hydrothermal condition. One method used titanium sulfate as precursor, while the other used titanium tetrachloride as precursor. The growth mechanism of titanium dioxide includes two reaction steps. The first reaction is the hydrolysis of titanium salt, in which polynuclear species of hydrous titania are formed. The second reaction represents the crystallizing reaction under hydrothermal condition, in which various polynuclear hydrous titania are combined together through dehydration reaction to form titanium dioxide crystals.
引用
收藏
页码:1445 / 1448
页数:4
相关论文
共 50 条
  • [31] The preparation and characterization of one-dimensional TiO2 nanostructure by hydrothermal method
    Yu, Lin
    Xu, Yuan-Yuan
    Zhao, Jing
    Xiao, Jin
    Xu, Wei-Long
    INTERNATIONAL JOURNAL OF MODERN PHYSICS B, 2020, 34 (1-3):
  • [32] Preparation, Characterization and Hydrothermal Stability of Hydrophobic TiO2/SiO2 Membrane
    Wang, Xiaohuan
    Yang, Jing
    Wang, Xuntao
    Zhang, Ruifeng
    Cui, Xinshui
    Wang, Nan
    Song, Jinghua
    INTEGRATED FERROELECTRICS, 2023, 234 (01) : 126 - 142
  • [33] Hydrothermal synthesis of brookite TiO2 nanoparticles for dye-sensitized solar cell
    Ezema, C. G.
    Nwanya, A. C.
    Ezema, B. E.
    Maaza, Malik
    Ukoha, P. O.
    Ezema, F. I.
    JOURNAL OF SOLID STATE ELECTROCHEMISTRY, 2017, 21 (09) : 2655 - 2663
  • [34] Microwave-driven polyol method for preparation of TiO2 nanocrystallites
    Yamamoto, T
    Wada, Y
    Yin, HB
    Sakata, T
    Mori, H
    Yanagida, S
    CHEMISTRY LETTERS, 2002, (10) : 964 - 965
  • [35] Preparation of TiO2 nanocrystallites by hydrolyzing with gaseous water and their photocatalytic activity
    Wang, ZL
    Mao, LQ
    Lin, J
    JOURNAL OF PHOTOCHEMISTRY AND PHOTOBIOLOGY A-CHEMISTRY, 2006, 177 (2-3) : 261 - 268
  • [36] Simple and effective preparation and characterization of nitrogen-doped TiO2 nanocrystallites and their visible light activities
    Cai, He-Shan
    Liu, Guo-Guang
    Li, Xiao-Xia
    Gongneng Cailiao/Journal of Functional Materials, 2012, 43 (13): : 1669 - 1672
  • [37] Preparation and photoactivity of nanostructured anatase, rutile and brookite TiO2 thin films
    Addamo, Maurizio
    Bellardita, Marianna
    Di Paola, Agatino
    Palmisano, Leonardo
    CHEMICAL COMMUNICATIONS, 2006, (47) : 4943 - 4945
  • [38] Direct synthesis of brookite-type titanium oxide by hydrothermal method using water-soluble titanium complexes
    Kobayashi, Makoto
    Tomita, Koji
    Petrykin, Valery
    Yoshimura, Masahiro
    Kakihana, Masato
    JOURNAL OF MATERIALS SCIENCE, 2008, 43 (07) : 2158 - 2162
  • [39] Preparation of brookite phase TiO2 colloidal sol for thin film coating
    Kim, SJ
    Lee, K
    Kim, JH
    Lee, NH
    Kim, SJ
    MATERIALS LETTERS, 2006, 60 (03) : 364 - 367
  • [40] Rapid Hydrothermal Preparation of Rutile TiO2 Nanoparticles by Simultaneous Transformation of Primary Brookite and Anatase: An in Situ Synchrotron PXRD Study
    Mi, Jian-Li
    Clausen, Casper
    Bremholm, Martin
    Lock, Nina
    Jensen, Kirsten M. O.
    Christensen, Mogens
    Iversen, Bo B.
    CRYSTAL GROWTH & DESIGN, 2012, 12 (12) : 6092 - 6097