Solid-phase synthesis of zinc(II) β-diketonates upon mechanical activation

被引：0
|
作者：
Petrova, LA [1 ]
Borisov, AP [1 ]
Makhaev, VD [1 ]
机构：
[1] Russian Acad Sci, Inst Problems Chem Phys, Chernogolovka 142432, Moscow Oblast, Russia
来源：
RUSSIAN JOURNAL OF INORGANIC CHEMISTRY | 2002年 / 47卷 / 12期
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D O I：
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中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Mechanically activated solid-phase reactions between zinc chloride and sodium beta-diketonates are studied. The course of the reaction, the product yield, and some properties of the activated mixtures are studied in relation to mechanical treatment conditions and the nature of beta-diketone. Zinc beta-diketonates are separated by sublimation from the activated mixtures in >70% yield. Unsolvated zinc beta-diketonates are characterized by physicochemical methods.
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页码：1827 / 1832
页数：6
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