Methyl acetate hydrolysis in a reactive divided wall column

被引:59
|
作者
Sander, S.
Flisch, C.
Geissier, E.
SchoenmakerS, H.
Ryll, O.
Hasse, H.
机构
[1] Sulzer Chemtech Ltd, CH-8404 Winterthur, Switzerland
[2] BASF AG, D-6700 Ludwigshafen, Germany
[3] Univ Stuttgart, Inst Thermodynam & Thermal Proc Engn, D-7000 Stuttgart, Germany
来源
关键词
methyl acetate hydrolysis; reactive divided wall column; reactive distillation;
D O I
10.1205/Cherd06106
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
The combination of reactive distillation and a divided wall column leads to a reactive divided wall column. The first use of such a reactive divided wall column for the hydrolysis of methyl acetate is presented here. For the development of this system, kinetic data for the involved reactions was determined at the University of Stuttgart, mini plant experiments were performed at BASF and an industrial scale column with an inner diameter of 220 mm was run at Sulzer Chemtech. Results of one mini plant experiment and of one experiment in an industrial scale are shown.
引用
收藏
页码:149 / 154
页数:6
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