Zeolite from fly ash: synthesis and characterization

被引：231
|
作者：
Ojha, K [1 ]
Pradhan, NC [1 ]
Samanta, AN [1 ]
机构：
[1] Indian Inst Technol, Dept Chem Engn, Kharagpur 721302, W Bengal, India
来源：
BULLETIN OF MATERIALS SCIENCE | 2004年 / 27卷 / 06期
关键词：
fly ash; NaX zeolite; hydrothermal treatment; X-ray diffraction; scanning electron microscopy; BET surface area;
D O I：
10.1007/BF02707285
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Coal fly ash was used to synthesize X-type zeolite by alkali fusion followed by hydrothermal treatment. The synthesized zeolite was characterized using various techniques such as X-ray diffraction, scanning electron microscopy, Fourier transform infrared spectroscopy, BET method for surface area measurement etc. The synthesis conditions were optimized to obtain highly crystalline zeoIite with maximum BET surface area. The maximum surface area of the product was found to be 383 m(2)/g with high purity. The crystallinity of the prepared zeolite was found to change with fusion temperature and a maximum value was obtained at 823 K. The cost of synthesized zeolite was estimated to be almost one-fifth of that of commercial 13X zeolite available in the market.
引用
收藏
页码：555 / 564
页数：10
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