Synthesis and characterization of bismuth titanate by an aqueous sol-gel method

被引：21
|
作者：
Du, Xianfeng [1 ]
Xu, Youlong [1 ]
Ma, Hanxiao [1 ]
Wang, Jie [1 ]
Li, Xifei [1 ]
机构：
[1] Xi An Jiao Tong Univ, Sch Elect & Informat Engn, Xian 710049, Peoples R China
来源：
JOURNAL OF THE AMERICAN CERAMIC SOCIETY | 2007年 / 90卷 / 05期
关键词：
D O I：
10.1111/j.1551-2916.2007.01548.x
中图分类号：
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号：
0805 ; 080502 ;
摘要：
A highly stable, reproducible and water-based bismuth titanate (BTO) sol system has been synthesized by an aqueous sol-gel method. First bismuth nitrate was dissolved in acetic acid, and then it was mixed with a solution of lactic acid dissolved tetra-n-butyl titanate, subsequently, water was added to adjust sol concentration. As-obtained sols or gels were characterized by Ultraviolet-Visible Spectrophotometer, derivative differential thermal analysis-differential thermal analysis-thermal gravimetry, in situ Raman, and high-temperature X-ray diffraction. Results show that the BTO sol can remain stable for more than 1 year and BTO can start to crystallize at about 450 degrees C.
引用
收藏
页码：1382 / 1385
页数：4
相关论文
共 50 条
  • [31] Synthesis and characterization of TiC powders by sol-gel method
    Gao, Liang
    Zhang, Yun
    Yang, Xue
    He, YanBin
    Song, LiHua
    JOURNAL OF CERAMIC PROCESSING RESEARCH, 2020, 21 (06): : 615 - 621
  • [32] Sol-gel prepared bismuth titanate for high temperature ultrasound transducers
    Burrows, S. E.
    McAughey, K. L.
    Edwards, R. S.
    Dixon, S.
    RSC ADVANCES, 2012, 2 (09): : 3678 - 3683
  • [33] Effect of Dysprosium Substitution on the Properties of Bismuth Titanate Thin Films Prepared by Sol-Gel Method
    Kao, M. C.
    Chen, H. Z.
    Young, S. L.
    Yu, C. C.
    Lin, C. H.
    Lin, C. C.
    Lee, C. M.
    FERROELECTRICS, 2009, 382 : 182 - 186
  • [34] Crystallization process of lanthanum-substituted bismuth titanate synthesized by a facile sol-gel method
    Ke, Hua
    Wang, Wen
    Chen, Lin
    Xu, Jiahuan
    Jia, Dechang
    Lu, Zhe
    Zhou, Yu
    JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY, 2010, 53 (01) : 135 - 140
  • [35] Synthesis of lead titanate nanoparticles via sol-gel technique and its characterization
    Sagadevan, Suresh
    Das, Isha
    Podder, Jiban
    JOURNAL OF MATERIALS SCIENCE-MATERIALS IN ELECTRONICS, 2016, 27 (12) : 13016 - 13021
  • [36] Synthesis and characterization of lead strontium titanate thin films by sol-gel technique
    Jain, M
    Majumder, SB
    Guo, R
    Bhalla, AS
    Katiyar, RS
    MATERIALS LETTERS, 2002, 56 (05) : 692 - 697
  • [37] Sol-gel synthesis and structural characterization of Fe doped barium titanate nanoceramics
    Tihtih, Mohammed
    Limame, Karoum
    Ababou, Yahya
    Sayouri, Salaheddine
    Ibrahim, Jamal-Eldin R. M.
    EPITOANYAG-JOURNAL OF SILICATE BASED AND COMPOSITE MATERIALS, 2019, 71 (06): : 190 - 193
  • [38] Characterization of nickel titanate synthesized by sol-gel processing
    Taylor, DJ
    Fleig, PF
    Page, RA
    THIN SOLID FILMS, 2002, 408 (1-2) : 104 - 110
  • [39] Synthesis and characterization of dense, monolithic gel derived by sol-gel method
    Matsuda, H
    Kobayashi, T
    Kuwabara, M
    Shimooka, H
    Takahashi, S
    CERAMIC PROCESSING SCIENCE, 1998, 83 : 27 - 33
  • [40] A novel sol-gel method for the synthesis of γ-aluminium oxide:: development of the sol-gel transformation and characterization of the xerogel
    Kureti, S
    Weisweiler, W
    JOURNAL OF NON-CRYSTALLINE SOLIDS, 2002, 303 (02) : 253 - 261
12345