Synthesis and Optical Property of a New Zinc Complex Based on the Derivative of 2-(2′-Hydroxyphenyl)-1H-benzimidazole and Phenanthroline

被引：0

作者：

Yin Guo-Jie ^{[1
]}

Zhang Hao-Yu ^{[1
]}

Tian Wen-Jie ^{[1
]}

Zhao Dan ^{[1
]}

Zhang Bin ^{[2
]}

Chen Dong-Mei ^{[1
]}

机构：

[1] Luoyang Inst Sci & Technol, Sch Environm Engn & Chem, Luoyang 471023, Peoples R China

[2] Zhengzhou Univ, Coll Chem, Zhengzhou 450000, Peoples R China

来源：

CHINESE JOURNAL OF STRUCTURAL CHEMISTRY | 2021年 / 40卷 / 04期

关键词：

synthesis; proton transfer; intramolecular hydrogen bond; INTRAMOLECULAR PROTON-TRANSFER; EMISSION; LUMINESCENCE; 2-(2'-HYDROXYPHENYL)BENZIMIDAZOLE; BENZIMIDAZOLES; CHROMOPHORES; TAUTOMERISM; ROTAMERISM; FILMS;

D O I：

10.14102/j.cnki.0254-5861.2011-2941

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A novel zinc complex (ZnE) has been designed and synthesized based on the derivative of 2-(2'-hydroxyphenyl)-1-H-benzimidazole (HBI) and the neutral nitrogen-containing ligand (phen). The crystal of the title complex crystallizes in the monoclinic system, space group P2(1)/n with a = 10.2631(2), b = 34.2166(6), c = 11.4103(3) angstrom, beta = 96.771(2)degrees, M-r = 844.24, V = 3978.99(14) angstrom(3), Z = 4, the final R = 0.0400 and wR = 0.1001 for 8107 observed reflections (I > 2 sigma(I)). In the title complex, the free protonated phenoxide moiety (4-OH) is successfully retained to realize pseudo-intramolecular hydrogen bonds with the coordinated 0 atom from the other ligand.

引用

页码：487 / 494

页数：8

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