Fast Simple Determination of Oxygen in Reduced Graphene Oxide by Inert Gas Fusion Method

被引：1
|
作者：
Wang, Kuan [1 ]
Chen, Na [2 ]
Li, Bo [1 ]
Zheng, Wei [1 ]
Liang, Qinghua [1 ]
机构：
[1] Northwest Inst Nonferrous Met Res, Mat Anal & Testing Ctr, 96 Wei Yang Rd, Xian 710016, Shaanxi, Peoples R China
[2] Xian Modern Chem Res Inst, Xian 710065, Shaanxi, Peoples R China
来源：
CHEMISTRYSELECT | 2018年 / 3卷 / 30期
关键词：
Determination oxygen; Inert gas fusion method; Reduced graphene oxide; X-ray photoelectron spectroscopy; RAY PHOTOELECTRON-SPECTROSCOPY; LITHIUM ION BATTERIES; EXFOLIATED GRAPHITE; REDUCTION; ATMOSPHERE; MECHANISM; VACUUM; LAYER; FILMS; FUEL;
D O I：
10.1002/slct.201800623
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A new method that combines inert gas fusion with infrared spectrometric detection for fast simple determination of total oxygen in reduced graphene oxide (RGO) has been established in this paper. The whole analyzing process was introduced, including calibration, temperature selection and sample weight selection. The equation of calculation the oxygen content of RGO in this method was given. The precision of the new method has been verified by measurement of a RGO sample. The RGO after measurement was characterized by X-ray photoelectron spectroscopy (XPS). The relative standard deviation (RSD) of oxygen was 1.02%. The results were consistent with that obtained by the conventional classic method XPS. It has shown that the new method is accurate and efficient. The method of testing a RGO sample needs 140 s. The inert gas fusion-infrared method is a fast simple method.
引用
收藏
页码：8748 / 8751
页数：4
相关论文
共 50 条
  • [31] DETERMINATION OF VANADIUM AND OXYGEN IN VANADIUM OXIDES BY DIFFERENTIAL SPECTROPHOTOMETRY AND INERT GAS FUSION-GAS CHROMATOGRAPHY
    LANNING, EW
    WEBERLIN.RP
    ANALYTICAL CHEMISTRY, 1968, 40 (03) : 626 - &
  • [32] Determination of the surface oxygen contents of silicon nitride powder using an acid dissolution/inert-gas fusion method
    Watanabe, M
    Narukawa, A
    BUNSEKI KAGAKU, 2001, 50 (01) : 57 - 60
  • [33] Simple and Fast Approach for Synthesis of Reduced Graphene Oxide-MoS2 Hybrids for Room Temperature Gas Detection
    Kumar, Rajesh
    Dias, Wagner, Jr.
    Rubira, Rafael J. G.
    Alaferdov, Andrei V.
    Vaz, Alfredo R.
    Singh, Rajesh K.
    Teixeira, Silvio R.
    Constantino, Carlos J. L.
    Moshkalev, Stanislav A.
    IEEE TRANSACTIONS ON ELECTRON DEVICES, 2018, 65 (09) : 3943 - 3949
  • [34] DETERMINATON OF OXYGEN IN MIXED FLUORIDES BY INERT GAS FUSION
    POTTER, JL
    HEADY, HH
    MURPHY, JE
    ANALYTICAL CHEMISTRY, 1962, 34 (12) : 1635 - &
  • [35] Fast simple determination of nitrogen in reduced graphene oxide by pulse furnace heating combined with thermal conductivity detection technique
    Wang, Kuan
    Yang, Junhong
    Gao, Dongxu
    Zhang, Zhe
    MEASUREMENT, 2025, 242
  • [36] MACRODETERMINATION OF OXYGEN IN METAL OXIDES BY INERT GAS FUSION
    HOLT, BD
    STOESSEL, JE
    ANALYTICAL CHEMISTRY, 1964, 36 (07) : 1320 - &
  • [37] USE OF A PYROLYTIC BORON NITRIDE THIMBLE IN DETERMINING OXYGEN BY INERT GAS FUSION METHOD
    BECK, EJ
    CHAMBERS, WE
    ANALYTICA CHIMICA ACTA, 1968, 43 (02) : 348 - &
  • [38] Fast and Facile Preparation of Graphene Oxide and Reduced Graphene Oxide Nanoplatelets
    Shen, Jianfeng
    Hu, Yizhe
    Shi, Min
    Lu, Xin
    Qin, Chen
    Li, Chen
    Ye, Mingxin
    CHEMISTRY OF MATERIALS, 2009, 21 (15) : 3514 - 3520
  • [39] Simple method to determine the purity of an inert gas
    Rev Sci Instrum, 6 (2438):
  • [40] A simple method to determine the purity of an inert gas
    Mao, O
    Altounian, Z
    StromOlsen, JO
    REVIEW OF SCIENTIFIC INSTRUMENTS, 1997, 68 (06): : 2438 - 2441
12345