On-line mid-IR spectroscopy as a real-time approach in monitoring hydrogenation reactions

被引:14
|
作者
Marziano, I [1 ]
Sharp, DCA [1 ]
Dunn, PJ [1 ]
Hailey, PA [1 ]
机构
[1] Pfizer Ltd, Cent Res, Sandwich CT13 9NJ, Kent, England
关键词
D O I
10.1021/op000030m
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
The use of mid-IR. spectroscopy as a real-time monitoring tool for hydrogenation reactions is illustrated. This technique was used for both qualitative and quantitative purposes to monitor the hydrogenation of three different functional groups. The results show that this technique can be successfully used as an alternative to traditional off-line methods to monitor the reaction endpoint and the formation of impurities.
引用
收藏
页码:357 / 361
页数:5
相关论文
共 50 条
  • [21] On-line purge and trap for real-time water monitoring.
    Saridara, C
    Brukh, R
    Mitra, S
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2004, 227 : U103 - U103
  • [22] ON-LINE, REAL-TIME INSTRUMENTATION FOR DIESEL PARTICULATE MONITORING.
    Patashnick, Harvey
    Textile Chemist and Colorist, 1987, 19 (10):
  • [23] Real-time biological process optimization using on-line monitoring
    Buttz, J.
    Daigger, G.
    Proceedings of the International Association on Water Pollution Research and Control (IAWPRC) Workshop, 1990,
  • [24] On-line and real-time monitoring of organophilic pervaporation by mass spectrometry
    Brazinha, Carla
    Fonseca, A. P.
    Teodoro, O. M. N. D.
    Crespo, Joao G.
    JOURNAL OF MEMBRANE SCIENCE, 2010, 347 (1-2) : 83 - 92
  • [25] Real-Time Tracking of Hot Carrier Injection at the Interface of FAPbBr3 Perovskite Using Femtosecond Mid-IR Spectroscopy
    Nadinov, Issatay
    Almasabi, Khulud
    Gutierrez-Arzaluz, Luis
    Thomas, Simil
    Hasanov, Bashir E.
    Bakr, Osman M.
    Alshareef, Husam N.
    Mohammed, Omar F.
    ACS CENTRAL SCIENCE, 2023, 10 (01) : 43 - 53
  • [26] Kinetic investigation of the living cationic polymerization of isobutylene with real-time monitoring using a mid-ir fiber optic probe.
    Kim, K
    Puskas, JE
    Rohani, S
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2002, 223 : D30 - D31
  • [27] Optimisation of SFE method on-line coupled to FT-IR spectroscopy for the real-time monitoring of the extraction of tagitinin C in T-diversifolia
    Ziemons, E.
    Mbakop, N. Wandji
    Rozet, E.
    Lejeune, R.
    Angenot, L.
    Thunus, L.
    Hubert, Ph.
    JOURNAL OF SUPERCRITICAL FLUIDS, 2007, 40 (03): : 368 - 375
  • [28] Real-time monitoring of nitrile biotransformations by mid-infrared spectroscopy
    Dadd, MR
    Sharp, DCA
    Pettman, AJ
    Knowles, CJ
    JOURNAL OF MICROBIOLOGICAL METHODS, 2000, 41 (01) : 69 - 75
  • [29] NIR spectroscopy as a process analytical technology (PAT) tool for on-line and real-time monitoring of an extraction process
    Wu, Yongjiang
    Jin, Ye
    Li, Yerui
    Sun, Di
    Liu, Xuesong
    Chen, Yong
    VIBRATIONAL SPECTROSCOPY, 2012, 58 : 109 - 118
  • [30] On-line fermentation monitoring by mid-infrared spectroscopy
    Mazarevica, G
    Diewok, J
    Baena, JR
    Rosenberg, E
    Lendl, B
    APPLIED SPECTROSCOPY, 2004, 58 (07) : 804 - 810