The structure of N-allyl-(5-phenyl-[1,3,4]thiadiazol-2-yl) amine in solution and the solid state studied by the 1H, 13C, 15N NMR spectroscopy and X-ray crystallography

被引：9
|
作者：
Strzemecka, Leokadia [1 ]
Urbanczyk-Lipkowska, Zofia [2 ]
机构：
[1] Med Univ Lublin, Dept Organ Chem, Fac Pharm, Med Analyt Div, PL-20081 Lublin, Poland
[2] Polish Acad Sci, Inst Organ Chem, PL-01224 Warsaw, Poland
来源：
JOURNAL OF MOLECULAR STRUCTURE | 2010年 / 970卷 / 1-3期
关键词：
Allyl-(5-phenyl-[1,3,4]thiadiazol-2-yl)-amine; H-1; C-13 N-15 NMR spectra; X-ray crystallography; CARBONIC-ANHYDRASE; ANTITUMOR-ACTIVITY; ALLYL DERIVATIVES; INHIBITORS; 2-ACYLAMINO-1,3,4-THIADIAZOLES; TAUTOMERISM;
D O I：
10.1016/j.molstruc.2009.05.016
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
The N-allyl-(5-phenyl-[1,3,4]thiadiazol-2-yl) amine was examined by the H-1, C-13, N-15 NMR spectroscopy and X-ray diffraction. It has been found that compound exists in the egzo-amino tautomeric form a in a solid state. The polar ribbons are observed in its crystal structure. (C) 2009 Elsevier B.V. All rights reserved.
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页码：1 / 13
页数：13
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