N-(2-Chlorobenzoyl)benzenesulfonamide

被引：5

作者：

Gowda, B. Thimme ^{[1
]}

Foro, Sabine ^{[2
]}

Suchetan, P. A. ^{[1
]}

Fuess, Hartmut ^{[2
]}

机构：

[1] Mangalore Univ, Dept Chem, Mangalagangothri 574199, Karnataka, India

[2] Tech Univ Darmstadt, Inst Mat Sci, D-64287 Darmstadt, Germany

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷

关键词：

Data-to-parameter ratio = 15.4; Disorder in main residue; Mean σ(C-C) = 0.004 Å; R factor = 0.041; Single-crystal X-ray study; T = 299 K; WR factor = 0.113;

D O I：

10.1107/S1600536809055482

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The asymmetric unit of the title compound, C(13)H(10)ClNO(3)S, contains two independent molecules, the chlorophenyl ring of one of them being disordered over two orientations with occupancies of 0.836 (2) and 0.164 (2). In one of the independent molecules, the sulfonyl-bound phenyl ring and the chlorophenyl ring form dihedral angles of 87.3 (1) and 46.8 (1)degrees, respectively, with the -S-NH-C=O segment, while in the other molecule the corresponding angles are 76.0 (1) and 39.6 (1)degrees. In the crystal, molecules are linked into tetrameric units by N-H center dot center dot center dot O hydrogen bonds.

引用

页码：O326 / U2130

页数：12

共 50 条

[41] Crystal structure of N-[3-(2-chlorobenzoyl)-5-ethylthiophen-2-yl]-2-[(E)-(2-hydroxybenzylidene) amino] acetamide
Kaur, Manpreet
Jasinski, Jerry P.
Kavitha, Channappa N.
Yathirajan, Hemmige S.
Byrappa, K.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O1011 - +
[42] N-(4-Chlorobenzoyl)-2-methylbenzenesulfonamide
Suchetan, P. A.
Gowda, B. Thimme
Foro, Sabine
Fuess, Hartmut
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1997 - U1022
[43] N-(3-Chlorobenzoyl)-2-nitrobenzenesulfonamide
Suchetan, P. A.
Foro, Sabine
Gowda, B. Thimme
Prakash, M. Shet
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O786 - U2604
[44] N-(3-Chlorobenzoyl)-2-methylbenzenesulfonamide
Suchetan, P. A.
Foro, Sabine
Gowda, B. Thimme
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O3489 - U790
[45] Crystal structure of N-[4-bromo-2-(2-chlorobenzoyl)phenyl]-2-chloroacetamide, C15H10BrCl2NO2
Kaur, Manpreet
Yathirajan, Hemmige S.
Dayananda, Alaloor S.
Gerber, Thomas
Hosten, Eric
Betz, Richard
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2013, 228 (01): : 113 - 114
[46] Synthesis, characterization and antimicrobial activities of transition metal complexes of N,N-dialkyl-N′-(2-chlorobenzoyl)thiourea derivatives
Binzet, Gun
Arslan, Hakan
Floerke, Ulrich
Kuelcue, Nevzat
Duran, Nizami
JOURNAL OF COORDINATION CHEMISTRY, 2006, 59 (12) : 1395 - 1406
[47] N-(5-Chloro-2-methoxyphenyl)benzenesulfonamide
Aziz-ur-Rehman
Shahzaman
Akkurt, Mehmet
Abbasi, Muhammad Athar
Khan, Islam Ullah
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O2855 - U532
[48] 4-Chloro-N-(3-chlorobenzoyl)benzenesulfonamide monohydrate
Suchetan, P. A.
Gowda, B. Thimme
Foro, Sabine
Fuess, Hartmut
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1773 - U320
[49] N-(4-chlorobenzoyl)-N′,N′-diethylthiourea
McKenzie, Jean M.
Koch, Klaus R.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O4263 - O4264
[50] N-(4-Methylbenzyl)-N-(6-methyl-2-pyridyl)benzenesulfonamide
Caylak, Nagihan
Hoekelek, Tuncer
Hasirci, Serdar
Erguen, Yavuz
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O2261 - O2262

← 1 2 3 4 5 →