Tetraphenyltetrabenzoporphyrinates of Ni(II), Pd(II), Pt(II) and Pt(IV)

被引：4
|
作者：
Maltceva, Olga V. [1 ]
Chizhova, Natalya V. [1 ]
Kumeev, Roman S. [1 ]
Mamardashvili, Nugzar Zh. [1 ]
机构：
[1] Russian Acad Sci, GA Krestov Inst Solut Chem, Ivanovo 153045, Russia
来源：
MACROHETEROCYCLES | 2017年 / 10卷 / 01期
关键词：
Synthesis; tetraphenyltetrabenzoporphyrinate; H-1 NMR spectroscopy; electron absorption spectroscopy; mass-spectrometry; elemental analysis; COMPLEXES; TETRABENZOPORPHYRINS;
D O I：
10.6060/mhc160541c
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The metal exchange reaction of 5,10,15,20-tetraphenyltetrabenzoporphyrinate of Cd(II) with Ni(II), Pd(II) and Pt(II) chlorides in DMF and phenol was investigated. Corresponding porphyrinates of Ni(II), Pd(II) and Pt(II) were obtained. 5,10,15,20-Tetraphenyltetrabenzoporphyrinate Pt(IV)(Br)(2) was synthesized through direct addition of Br 2 to the porphyrinate Pt(II) in chloroform. The prepared compounds were identified by the methods of electronic absorption, H-1 NMR spectroscopy, mass spectrometry and elemental analysis.
引用
收藏
页码：68 / 71
页数：4
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