Synthesis and crystal structure of the zinc(II) coordination polymer with 1,1-(1,4-butanediyl)bis(imidazole)

被引：0
|
作者：
Chen, F. [1 ,2 ]
Pan, D. -H. [1 ]
Xu, Y. -P. [1 ]
Yang, R. -L. [1 ]
Wang, L. -Z. [1 ]
Yang, M. [1 ]
Luo, S. -N. [1 ,2 ]
机构：
[1] Jiangsu Inst Nucl Med, Jiangsu Key Lab Mol Nucl Med, Minist Hlth, Key Lab Nucl Med, Wuxi 214063, Jiangsu, Peoples R China
[2] Nanjing Med Univ, Nanjing 210029, Jiangsu, Peoples R China
来源：
CRYSTALLOGRAPHY REPORTS | 2014年 / 59卷 / 07期
基金：
中国博士后科学基金;
关键词：
LUMINESCENT PROPERTIES; LIGANDS; COMPLEXES; 1,3,5-BENZENETRICARBOXYLATE; BIS(IMIDAZOLE); CADMIUM(II); TOPOLOGIES; ANION;
D O I：
10.1134/S1063774514070074
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The self-assembly of 1,1-(1,4-butanediyl)bis(imidazole) (L) with [ZnL(NO3)(2)] gives the new coordination polymer C10H14N6O6Zn (1). The crystal structure of 1 was determined by X-ray diffraction. It crystallizes in space group with a = 7.9975(11), b = 8.4392(11), c = 13.8326(19) ; alpha = 76.876(2)A degrees, beta = 85.892(2)A degrees, gamma = 71.0440(10)A degrees and Z = 2. In the complex, Zn atom is coordinated to two nitrogen atoms from two molecules of L and to two oxygen atoms from two nitrate groups. Each L molecule is coordinated to two Zn atom, acting as a bridging ligand. The Zn-N bond lengths are 1.995(3) and 2.014(2) , and Zn-O bond lengths are 1.944(2) and 1.958(3) angstrom.
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收藏
页码：1010 / 1012
页数：3
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