Microwave-assisted solvent-free parallel synthesis of thioamides

被引：45
|
作者：
Olsson, R [1 ]
Hansen, HC [1 ]
Andersson, CM [1 ]
机构：
[1] ACADIA Pharmaceut AS, Synthet Chem, DK-2600 Glostrup, Denmark
来源：
TETRAHEDRON LETTERS | 2000年 / 41卷 / 41期
关键词：
microwave; parallel synthesis; thioamide;
D O I：
10.1016/S0040-4039(00)01360-5
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Rapid parallel synthesis of thioamides is described. A library of amides, synthesised by mixing acyl chlorides and diamines, was transformed into the corresponding thioamides utilising Lawesson's reagent as the oxygen/sulphur exchange reagent. Purification by solid-phase extraction afforded the library members in adequate purities and yields. (C) 2000 Elsevier Science Ltd. All rights reserved.
引用
收藏
页码：7947 / 7950
页数：4
相关论文
共 50 条
  • [41] Microwave-assisted synthesis of photochromic spirooxazine dyes under solvent-free condition
    Lee, CC
    Wang, JC
    Hu, AT
    [J]. MATERIALS LETTERS, 2004, 58 (3-4) : 535 - 538
  • [42] Efficient microwave-assisted synthesis of quinolines and dihydroquinolines under solvent-free conditions
    Ranu, BC
    Hajra, A
    Dey, SS
    Jana, U
    [J]. TETRAHEDRON, 2003, 59 (06) : 813 - 819
  • [43] SYNTHESIS OF NOVEL CINNAMOYL AMIDES USING A SOLVENT-FREE MICROWAVE-ASSISTED METHOD
    Pellon, Rolando F.
    Docampo, Maite L.
    [J]. SYNTHETIC COMMUNICATIONS, 2013, 43 (04) : 537 - 552
  • [44] Microwave-assisted synthesis of quinoxalines, benzoxazines, and benzothiazines under solvent-free conditions
    Heravi, MM
    Nami, N
    Oskooie, HA
    Hekmatshoar, R
    [J]. PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2005, 180 (08) : 1873 - 1878
  • [45] Microwave-assisted silica-promoted solvent-free synthesis of triazoloquinazolinone and benzimidazoquinazolinones
    Krishnamurthy G.
    Jagannath K.V.
    [J]. Journal of Chemical Sciences, 2013, 125 (4) : 807 - 811
  • [46] Solvent-free microwave-assisted aromatic nucleophilic substitution - Synthesis of aromatic ethers
    Chaouchi, M
    Loupy, A
    Marque, S
    Petit, A
    [J]. EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2002, 2002 (07) : 1278 - 1283
  • [47] Microwave-Assisted Solvent-Free Synthesis of Quinolines Using N-Bromosulfonamides
    Ghorbani-Vaghei, Ramin
    Akbari-Dadamahaleh, Somayeh
    [J]. PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2010, 185 (02) : 319 - 324
  • [48] Solvent-free catalyst-free microwave-assisted acylation of lignin
    Monteil-Rivera, Fanny
    Paquet, Louise
    [J]. INDUSTRIAL CROPS AND PRODUCTS, 2015, 65 : 446 - 453
  • [49] Microwave-assisted Wurtz coupling of methylphenyldichlorosilane in solvent-free conditions
    Sacarescu, Gabriela
    Simionescu, Mihaela
    Harabagiu, Valeria
    Sacarescu, Liviu
    [J]. E-POLYMERS, 2012,
  • [50] Microwave-Assisted Passerini Reactions under Solvent-Free Conditions
    Barreto, Angelica de Fatima S.
    Vercillo, Otilie E.
    Andrade, Carlos Kleber Z.
    [J]. JOURNAL OF THE BRAZILIAN CHEMICAL SOCIETY, 2011, 22 (03) : 462 - 467
12345