Analysis of carbon in archaeological glass and pottery by low energy deuteron activation technique

被引:1
|
作者
Sastri, Chaturvedula S. [1 ]
Sauvage, Thierry [2 ]
Blondiaux, Gilbert [3 ]
Wendling, Olivier [2 ]
Bellamy, Aurelien [2 ]
Humburg, Christian [4 ]
机构
[1] Michael Mueller Ring 29, D-55128 Mainz, Germany
[2] CNRS CEMHTI, Site Cyclotron, 3A Rue Ferollerie, F-45071 Orleans 2, France
[3] 2 Rue Moissons, F-05000 Gap, France
[4] Zeppelin Str 25, D-55131 Mainz, Germany
关键词
Activation analysis; Charged particles; Deuterons; Positron emitters; Gamma-ray spectroscopy; Decay-curve analysis; CERAMIC MATERIALS; OXYGEN DETERMINATION; NITROGEN; RECONSTRUCTION; ALUMINUM; METALS;
D O I
10.1007/s10967-021-07820-x
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Carbon in archaeological glass and pottery is determined in a simple and elegant way by deuteron activation based on C-12(d,n)N-13 nuclear reaction. The method is rapid, non-destructive and carbon result is obtained along with Na, Mg, Al and Cl in a single irradiation. In the wood-fired Roman furnaces, carbon entered the glass melt probably through fumes and/or alkali plant-ash flux. Carbon is found in the range of 1300 to 4400 (mu g/g) in glass. The theoretical detection limit of 5 mu g/g is difficult to achieve because of higher carbon blank from the environment/atmosphere.
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页码:889 / 897
页数:9
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