O,O′-Ditolyldithiophosphates of Zinc(II), Cadmium(II) and Mercury(II)

被引：0

作者：

Kour, Simerpal ^{[1
]}

Gupta, Bhawana ^{[1
]}

Chander, Romesh ^{[1
]}

Pandey, Sushil Kumar ^{[1
]}

机构：

[1] Univ Jammu, Dept Chem, Jammu 180006, Jammu & Kashmir, India

来源：

MAIN GROUP METAL CHEMISTRY | 2009年 / 32卷 / 04期

关键词：

Metallo-organic; Phosphorus compounds; Ditolyldithiophosphates; Dialkyl-/alkylenedithiophosphates; CRYSTAL-STRUCTURE; DITHIOPHOSPHATE; DERIVATIVES; CHEMISTRY; DIALKYL; P-31;

D O I：

暂无

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

O,O'-Ditolyldithiophosphato complexes of zinc(II), cadmium(II) and mercury(II) corresponding to [(CreO)(2)PS2](2)M (CreO = o-, m- and p-CH3C6H4 and M = Zn, Cd and Hg) have been synthesized by the reaction of metal dichlorides, MCl2, with triethylammonium O,O'-ditolylphosphorodithioate, (o-, m- and p-CH3C6H4O)(2)PS2HNEt3, in 1:2 molar stoichiometry tinder anhydrous conditions These complexes were characterized by elemental analyses, molecular weight determination, IR and NMR (H-1, C-13 and P-31) spectral studies, which revealed monomeric nature of these complexes and the metal atom being four-coordinatively bonded to two bidentate dithiophosphate ligands, leading to a square plannar geometry around the metal atom

引用

页码：195 / 202

页数：8

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