Reaction of 2-acetyl-5-methyl-2H-1,2,3-diazaphosphole with butane-2,3-diol

被引：9

作者：

Khusainova, NG ^{[1
]}

Mostovaya, OA

Azancheev, NM

Litvinov, IA

Krivolapov, DB

Cherkasov, RA

机构：

[1] Kazan VI Lenin State Univ, Dept Chem, Kazan 420008, Russia

[2] Russian Acad Sci, AE Arbuzov Organ & Phys Chem Inst, Kazan Sci Ctr, Kazan 420088, Russia

来源：

MENDELEEV COMMUNICATIONS | 2004年 / 14卷 / 05期

关键词：

D O I：

10.1070/MC2004v014n05ABEH001926

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The reaction of 2-acetyl-5-methyl-2H-1,2,3-diazaphosphole with (rac)-butane-2,3-diol at temperatures below 0 degreesC leads to the formation of a hydrospirophosphorane containing both a diazaphospholene and a dioxaphospholane ring system and a beta-hydroxyalkoxy-1,2,3-diazaphospholene. On heating, these products form a hydrospirotetraoxaphosphorane, its tautomeric monocyclic beta-hydroxyalkylphosphite and N-acetyl-N'-isopropylidene-hydrazine.

引用

页码：212 / 214

页数：3

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