Effect of pH value on structural and magnetic properties of CuFe2O4 nanoparticles synthesized by low temperature hydrothermal technique

被引:56
|
作者
Ramaprasad, T. [1 ,2 ,3 ]
Kumar, R. Jeevan [1 ]
Naresh, U. [1 ]
Prakash, M. [1 ]
Kothandan, D. [4 ]
Naidu, K. Chandra Babu [5 ]
机构
[1] Sri Krishnadevaraya Univ, Dept Phys, Anantapuramu, AP, India
[2] MRITS, Hyderabad, Telangana, India
[3] Rayalaseema Univ, Dept Phys, Kurnool, AP, India
[4] Sreenivasa Inst Technol & Management Sci, Chittoor, AP, India
[5] GITAM Deemed Be Univ, Dept Phys, Bangalore, Karnataka, India
来源
MATERIALS RESEARCH EXPRESS | 2018年 / 5卷 / 09期
关键词
nanoparticles; structure; magnetic properties; hydrothermal synthesis; INITIAL PERMEABILITY; MICROWAVE; FERRITES; CATIONS;
D O I
10.1088/2053-1591/aad860
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The present study deals with the effect of pH value on structural and magnetic properties of copper ferrite (CF) nanoparticles synthesized via low temperature hydrothermal approach. In particular, the pH is varied from 9 to 12, in order to elucidate the behavior of structural, morphological, magnetic and optical properties of CF nanoparticles. The diffraction pattern revealed the formation of mixed (cubic & tetragonal) phase and cubic single phase structure. Later on, the structure, average crystallite size (D), grain size (G), particle size, saturation magnetization (Ms), anisotropy constant (K-1), magnetic moment (miB), octahedral (nu(1)) & tetrahedral (nu(2)) locations are also evaluated. Moreover, the cation distribution was performed for all the samples. The superparamagnetic nature of CF nanoparticles is confirmed by M-H curves.
引用
收藏
页数:11
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