ARTEMIS, THE 14C AMS FACILITY OF THE LMC14 NATIONAL LABORATORY: A STATUS REPORT ON QUALITY CONTROL AND MICROSAMPLE PROCEDURES

被引：24

作者：

Moreau, Christophe ^{[1
]}

Messager, Cyrielle ^{[1
]}

Berthier, Bernard ^{[1
]}

Hain, Stephane ^{[1
]}

Thellier, Bruno ^{[1
]}

Dumoulin, Jean-Pascal ^{[1
]}

Caffy, Ingrid ^{[1
]}

Sieudat, Marc ^{[1
]}

Delque-Kolic, Emmanuelle ^{[1
]}

Mussard, Solene ^{[1
]}

Perron, Marion ^{[1
]}

Setti, Valerie ^{[1
]}

Beck, Lucile ^{[1
]}

机构：

[1] Univ Paris Saclay, LSCE IPSL, CEA CNRS UVSQ, Lab Mesure Carbone LMC14 14, Gif Sur Yvette, France

来源：

RADIOCARBON | 2020年 / 62卷 / 06期

关键词：

AMS; lead white painting; microsample; quality control procedures; radiocarbon dating; SMALL RADIOCARBON SAMPLES; GAS ION-SOURCE; SACLAY; CONTAMINATION; EXTRACTION; CARBON;

D O I：

10.1017/RDC.2020.73

中图分类号：

P3 [地球物理学]; P59 [地球化学];

学科分类号：

0708 ; 070902 ;

摘要：

Quality control procedures have been developed at the Laboratoire de Mesure du Carbone 14 (LMC14) national laboratory throughout the years of operation. Routine procedures are applied to sample preparation depending on their composition and their size. The tuning of the ARTEMIS AMS facility, hosted by the LMC14 laboratory, uses an accurate procedure. A batch of unknown samples is measured with accompanying samples (primary and secondary standards and blanks), which give a powerful set of data to control the quality of each measurement. A homemade database has been created to store the sample information and study the evolution of the accompanying samples. The LMC14 laboratory participated in the Sixth International Radiocarbon Intercomparison, SIRI. The results are presented here, with statistical tests to assess the quality of the preparations and measurements done at the LMC14 national laboratory. To obtain a reliable radiocarbon (C-14) age by AMS, 1 mg of sample is required in routine analysis. Recently, the LMC14 developed a new procedure dedicated to microsamples, allowing the size of samples to be reduced and contributing to opening C-14 dating to materials that were previously unreachable. This new procedure has been successfully tested on valuable Cultural Heritage samples: lead white mural paintings.

引用

页码：1755 / 1770

页数：16

共 42 条

[31] AMS measurements of 14C, 36Cl, and 239/240Pu samples taken in a 'small facility'
Michel, M.
Filby, A.
Heinze, S.
Margreiter, R.
Strub, E.
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS, 2022, 533 : 70 - 75
[32] The necessity of sample quality assessment in 14C AMS dating: The case of Cova des Pas (Menorca - Spain)
Van Strydonck, Mark
Boudin, Mathieu
Guerrero Ayuso, Victor M.
Calvo, Manuel
Fullola, Josep M.
Angeles Petit, M.
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS, 2010, 268 (7-8): : 990 - 994
[33] Is comparability of 14C dates an issue?:: A status report on the fourth international radiocarbon intercomparison
Bryant, C
Carmi, I
Cook, GT
Gulliksen, S
Harkness, DD
Heinemeier, J
McGee, E
Naysmith, P
Possnert, G
Scott, EM
van Strydonck, M
RADIOCARBON, 2001, 43 (2A) : 321 - 324
[34] Status report on sample preparation facilities for 14C analysis at the new CologneAMS center
Rethemeyer, J.
Fueloep, R. -H.
Hoefle, S.
Wacker, L.
Heinze, S.
Hajdas, I.
Patt, U.
Koenig, S.
Stapper, B.
Dewald, A.
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS, 2013, 294 : 168 - 172
[35] ENVIRONMICADAS: A MINI 14C AMS WITH ENHANCED GAS ION SOURCE INTERFACE IN THE HERTELENDI LABORATORY OF ENVIRONMENTAL STUDIES (HEKAL), HUNGARY
Molnar, M.
Rinyu, L.
Veres, M.
Seiler, M.
Wacker, L.
Synal, H-A
RADIOCARBON, 2013, 55 (2-3) : 338 - 344
[36] Naturally Dyed Wool and Silk and Their Atomic C:N Ratio for Quality Control of 14C Sample Treatment
Boudin, Mathieu
Bonafini, Marco
Berghe, Ina Vanden
Maquoi, Marie-Christine
RADIOCARBON, 2016, 58 (01) : 55 - 68
[37] Radiocarbon Laboratory at the National Autonomous University of Mexico:: First set of samples and new 14C internal reference material
Beramendi-Orosco, Laura E.
Gonzalez-Hernandez, Galia
Urrutia-Fucugauchi, Jaime
Morton-Bermea, Ofelia
RADIOCARBON, 2006, 48 (03) : 485 - 491
[38] The use of Raman spectroscopy to monitor the removal of humic substances from charcoal:: Quality control for 14C dating of charcoal
Alon, D
Mintz, G
Cohen, I
Weiner, S
Boaretto, E
RADIOCARBON, 2002, 44 (01) : 1 - 11
[39] A laboratory inter-comparison of AMS 14C dating of bones of the Miesenheim IV elk (Rhineland, Germany) and its implications for the date of updates the Laacher See eruption
Kuzmin, Yaroslav V.
Fiedel, Stuart J.
Street, Martin
Reimer, Paula J.
Boudin, Mathieu
van der Plicht, Johannes
Panov, Vsevolod S.
Hodgins, Gregory W. L.
QUATERNARY GEOCHRONOLOGY, 2018, 48 : 7 - 16
[40] ULTRA-SMALL GRAPHITIZATION REACTORS FOR ULTRA-MICROSCALE 14C ANALYSIS AT THE NATIONAL OCEAN SCIENCES ACCELERATOR MASS SPECTROMETRY (NOSAMS) FACILITY
Walter, Sunita R. Shah
Gagnon, Alan R.
Roberts, Mark L.
McNichol, Ann P.
Gaylord, Mary C. Lardie
Klein, Elizabeth
RADIOCARBON, 2015, 57 (01) : 109 - 122

← 1 2 3 4 5 →