Facile one-pot synthesis of nanoporous hypercrosslinked hydroxybenzene formaldehyde resins with high surface area and adjustable pore texture

被引：10
|
作者：
Zeng, Shao-Zhong [1 ]
Guo, Limin [1 ]
He, Qianjun [1 ]
Chen, Yu [1 ]
Jiang, Peng [1 ]
Shi, Jianlin [1 ]
机构：
[1] Chinese Acad Sci, Shanghai Inst Ceram, State Key Lab High Performance Ceram & Superfine, Shanghai 200050, Peoples R China
来源：
MICROPOROUS AND MESOPOROUS MATERIALS | 2010年 / 131卷 / 1-3期
关键词：
Hydroxybenzene; Hypercrosslinked; Nanostructure; Polymers; Synthetic methods; COVALENT ORGANIC FRAMEWORKS; INTRINSIC MICROPOROSITY PIMS; HYDROGEN STORAGE; POLYMERS; CRYSTALLINE; ADSORPTION; COPOLYMER; NETWORKS;
D O I：
10.1016/j.micromeso.2009.12.014
中图分类号：
O69 [应用化学];
学科分类号：
081704 ;
摘要：
Hydroxybenzene formaldehyde resins with high surface area (up to 1000 m(2) g(-1)), high pore volume (up to 2.4 cm(3) g(-1)) and adjustable pore size distribution have been synthesized by a facile one-pot method. The pore formation was confirmed to be a hypercrosslinked mechanism. These results extend the synthetic methods of hypercrosslinked polymers from conventional nonaqueous Friedel-Crafts condensation to aqueous phenol-aldehyde reaction. (C) 2009 Elsevier Inc. All rights reserved.
引用
收藏
页码：141 / 147
页数：7
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