Methyl 3,5-bis[(4-hydroxymethyl-2-methoxyphenoxy)methyl]benzoate

被引:0
|
作者
Arshad, Muhammad Nadeem [2 ]
Mough, Scott T. [1 ]
Goeltz, John C. [1 ]
Holman, K. Travis [1 ]
机构
[1] Georgetown Univ, Dept Chem, Washington, DC 20057 USA
[2] Govt Coll Univ, Dept Chem, Lahore 54000, Pakistan
基金
美国国家科学基金会;
关键词
Data-to-parameter ratio = 14.1; Mean σ(C-C) = 0.004 Å; R factor = 0.054; Single-crystal X-ray study; T = 173 K; WR factor = 0.128;
D O I
10.1107/S160053681000677X
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C26H28O8, the central aromatic ring forms dihedral angles of 24.32 (11) and 80.19 (7)degrees with the two adjoining vanillyl alcohol rings. In the crystal, O-H center dot center dot center dot O hydrogen bonds connect the molecules, forming a hydrogen-bonded sheet-like motif extended in the ab plane.
引用
收藏
页码:O703 / U5737
页数:12
相关论文
共 50 条
  • [21] Inhibition of migration of MDA-MB-231 cells by methyl-3,5-diiodo-4-(4'-methoxyphenoxy)benzoate (DIME)
    Buki, KG
    Kirsten, E
    Bauer, PI
    Vidair, CA
    Kun, A
    Mendeleyev, J
    Kun, E
    INTERNATIONAL JOURNAL OF ONCOLOGY, 1997, 11 (06) : 1247 - 1250
  • [22] METHYL 3,5-DIIODO-4-(3-ISOPROPYL-4-METHOXYBENZOYL)BENZOATE
    CODY, V
    CHEUNG, E
    JORGENSEN, EC
    ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1982, 38 (AUG): : 2270 - 2272
  • [23] 3,5-bis[(carbazol-9-yl)methyl]-1-methoxybenzene
    Kumar, G. Senthil
    Chinnakali, K.
    Sekar, K.
    Rajakumar, P.
    Fun, Hoong-Kun
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O3597 - O3599
  • [24] From small structural modifications to adjustment of structurally dependent properties: 1-methyl-3,5-bis[(E)-2-thienylidene]-4-piperidone and 3,5-bis[(E)-5-bromo-2-thienylidene]-1-methyl-4-piperidone
    Tongwa, Paul
    Kinnibrugh, Tiffany L.
    Kicchaiahgari, Geetha R.
    Khrustalev, Victor N.
    Timofeeva, Tatiana V.
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2009, 65 : O155 - O159
  • [25] STRUCTURES OF 2,6-BIS(BENZYLIDENE)CYCLOHEXANONE(III) AND 3,5-BIS(4-DIMETHYLAMINOBENZYLIDENE)-1-METHYL-4-PIPERIDONE(IV)
    JIA, ZC
    QUAIL, JW
    ARORA, VK
    DIMMOCK, JR
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1989, 45 : 285 - 289
  • [26] 1-(4-{[3,5-bis({[3,5-Dimethyl-4-(4-methyl-3,5-dioxo-1,2,4-triazolidin-1-yl)-phenoxy]methyl})phenyl]methoxy}-2,6-dimethyl-phenyl)-4-methyl-1,2,4-triazolidine-3,5-dione
    Breton, Gary W.
    Bowron Jr, James Alexander
    MOLBANK, 2023, 2023 (01)
  • [27] Synthesis of 3,5-Bis(hydroxymethyl)adamantan-1-ols and 3,5-Bis(nitrooxymethyl)adamantan-1-yl Nitrates
    Ivleva, E. A.
    Kazakova, A. I.
    Klimochkin, Yu. N.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2020, 56 (09) : 1562 - 1569
  • [28] 4,5-Bis(4-methoxyphenoxy)phthalonitrile
    Yu, Lijuan
    Zhou, Xiaole
    Yin, Yinghui
    Li, Renjie
    Peng, Tianyou
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O2527 - U171
  • [29] Synthesis of 3,5-Bis(hydroxymethyl)adamantan-1-ols and 3,5-Bis(nitrooxymethyl)adamantan-1-yl Nitrates
    E. A. Ivleva
    A. I. Kazakova
    Yu. N. Klimochkin
    Russian Journal of Organic Chemistry, 2020, 56 : 1562 - 1569
  • [30] Tetraethylammonium 2-[bis(4-hydroxyphenyl)methyl]benzoate
    Li, Xiaofei
    Tong, Yan
    Quah, Ching Kheng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O3148 - U673