An efficient synthesis of 3,4-dihydropyrimidin-2-ones catalyzed by NH2SO3H under ultrasound irradiation

被引：241
|
作者：
Li, JT [1 ]
Han, JF [1 ]
Yang, JH [1 ]
Li, TS [1 ]
机构：
[1] Hebei Univ, Coll Chem & Environm Sci, Baoding 071002, Peoples R China
来源：
ULTRASONICS SONOCHEMISTRY | 2003年 / 10卷 / 03期
关键词：
Biginelli reaction; dihydropyrimidinones; synthesis; ultrasound irradiation;
D O I：
10.1016/S1350-4177(03)00092-0
中图分类号：
O42 [声学];
学科分类号：
070206 ; 082403 ;
摘要：
The condensation of aldehydes, beta-keto esters and urea catalyzed by NH2SO3H in ethanol results dihydropyrimidinones in high yields under ultrasound irradiation. (C) 2003 Elsevier Science B.V. All rights reserved.
引用
收藏
页码：119 / 122
页数：4
相关论文
共 50 条
  • [41] Solvent-Free Biginelli Reaction: A Green Method for the Synthesis of 3,4-Dihydropyrimidin-2-ones Catalyzed by Protic Acids in Large-Scale
    Wang, Yangyun
    Yu, Jipan
    Yang, Haohao
    Miao, Zhiwei
    Chen, Ruyu
    LETTERS IN ORGANIC CHEMISTRY, 2011, 8 (04) : 264 - 267
  • [42] Synthesis of 3,4-dihydropyrimidin-2(1H)-ones catalyzed by poly(ferric 2-acrylamido-2-methylpropanesulfonate)
    Zhao, Zhihao
    Dai, Hongguang
    Shi, Lan
    CHEMICAL PAPERS, 2021, 75 (02): : 583 - 590
  • [43] Synthesis of 3,4-Dihydropyrimidin-2(1H)-ones, -thione, and -selones, Catalyzed by TiO2 Nanoparticles
    Mohammadi, B.
    Behbahani, F. K.
    Marandi, G. B.
    Mirza, B.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2022, 58 (09) : 1319 - 1326
  • [44] Synthesis of 3,4-dihydropyrimidin-2(1H)-ones catalyzed by poly(ferric 2-acrylamido-2-methylpropanesulfonate)
    Zhihao Zhao
    Hongguang Dai
    Lan Shi
    Chemical Papers, 2021, 75 : 583 - 590
  • [45] Synthesis of 3,4-Dihydropyrimidin-2(1H)-ones, -thione, and -selones, Catalyzed by TiO2 Nanoparticles
    B. Mohammadi
    F. K. Behbahani
    G. B. Marandi
    B. Mirza
    Russian Journal of Organic Chemistry, 2022, 58 : 1319 - 1326
  • [46] An efficient synthesis of 3,4-dihydorpymidine(1H)-(thio)-ones catalyzed by novel SO3H-functionalized ionic liquids under ultrasound irradiation and solvent free conditions
    Li, BaiLin
    Ge, ChangHua
    Ying, An Guo
    ADVANCED RESEARCH ON MATERIAL ENGINEERING, CHEMISTRY, BIOINFORMATICS II, 2012, 531 : 428 - 431
  • [47] One-pot synthesis of 3,4-dihydropyrimidin-2(1H)-ones catalyzed by SO3H@imineZCMNPs as a novel, efficient and reusable acidic nanocatalyst under solvent-free conditions
    Abbaspour-Gilandeh, Esmayeel
    Yahyazadeh, Asieh
    Aghaei-Hashjin, Mehraneh
    RSC ADVANCES, 2018, 8 (70) : 40243 - 40251
  • [48] Mn(OAc)3•2H2O-mediated three-component, one-pot, condensation reaction:: an efficient synthesis of 4-aryl-substituted 3,4-dihydropyrimidin-2-ones
    Kumar, KA
    Kasthuraiah, M
    Reddy, CS
    Reddy, CD
    TETRAHEDRON LETTERS, 2001, 42 (44) : 7873 - 7875
  • [49] *CONTRIBUTION A LETUDE DE LACIDE AMIDOSULFONIQUE (NH2SO3H)
    SAKELLARIDIS, P
    BULLETIN DE LA SOCIETE CHIMIQUE DE FRANCE, 1951, 18 (9-10): : 610 - 612
  • [50] Praseodymium methanesulfonate catalyzed one-pot synthesis of 3,4-dihydropyrimidin-2-(1H)-ones
    Wang, Min
    Song, Zhiguo
    Gong, Hong
    Jiang, Heng
    PREPARATIVE BIOCHEMISTRY & BIOTECHNOLOGY, 2008, 38 (01): : 105 - 114
12345