Synthesis of aromatic polycyclic benzofuroxan compounds

被引:0
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作者
Li, X [1 ]
Tian, Y [1 ]
机构
[1] CAEP, Inst Chem Mat, Chengdu 610003, Peoples R China
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中图分类号
O414.1 [热力学];
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摘要
Two benzofuroxan compounds, N,N'-bis (2',4'-dinitro-benzofuro xanyl) -1,3,5-trinitro-2,4-diaminobenzene and N, N', N "-tri (2', 4'-dinitro-benzofuroxanyl) -1, 3, 5-trinitro-2, 4, 6-triaminobenzene were synthesized from 2, 4-dichloro-1, 3, 5-trinitrobenzene, 2, 4, 6-trichloro-1, 3, 5-trinitrobenzene and 3-Chloroaniline through condensation,nitration, azidation and pyrolysis reactions. The molecular structures of the benzofuroxans and their intermediates were characterized by elemental analysis, IR, (HNMR)-H-1 and MS spectroscopy.
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页码:52 / 54
页数:3
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