Preparation of activated carbon from bamboo-cellulose fiber and its use for EDLC electrode material

被引:44
|
作者
Fujishige, Masatsugu [1 ]
Yoshida, Ichiro [1 ]
Toya, Yumiko [1 ]
Banba, Yasuo [1 ]
Oshida, Kyo-ichi [2 ]
Tanaka, Yu-suke [3 ]
Dulyaseree, Paweena [4 ]
Wongwiriyapan, Winadda [4 ]
Takeuchi, Kenji [1 ]
机构
[1] Shinshu Univ, Inst Carbon Sci & Technol, 4-17-1 Wakasato, Nagano 3808553, Japan
[2] Nagano Natl Coll Technol, 716 Tokuma, Nagano 3808550, Japan
[3] Shinshu Univ, Interdisciplinary Grad Sch Sci & Technol, 4-17-1 Wakasato, Nagano 3808553, Japan
[4] King Mongkuts Inst Technol Ladkrabang, Coll Nanotechnol, Chalongkrung Rd, Bangkok 10520, Thailand
来源
关键词
Bamboo; Cellulose fiber; Activated carbon; EDLC electrode; Carbonization; GRAPHITE; RAMAN; CARBONIZATION; SODIUM;
D O I
10.1016/j.jece.2017.03.011
中图分类号
X [环境科学、安全科学];
学科分类号
08 ; 0830 ;
摘要
Carbonization and post activation of bamboo-cellulose fiber was carried out. The carbonization was performed at 600 degrees C, 800 degrees C and 1000 degrees C in argon atmosphere. Then, they were activated by heating solid mixture of carbonized bamboo and sodium hydroxide (NaOH) at 720 degrees C in argon atmosphere. The largest specific surface area of the resulting activated carbon (carbonized at 600 degrees C) was 2366 m(2)/g with the micropore volume of 0.71 cm(3)/g and mesopore volume of 0.06 cm(3)/g. It was found that the carbonization temperature is very important to obtain nanoporous carbon with large specific surface area. The distributions of interlayer spacing were estimated from the power spectra of the TEM images of the carbonized samples. It showed the interlayer spacing of basic structural unit (BSU) decreased from 0.49 nm (BC-0600) through 0.47 nm (BC-0800) to 0.45 nm (BC-1000). The activated carbon was used as the host material of the electrodes of coin type electric double-layer capacitor (EDLC) with organic electrolyte. The observed specific capacitance was 43 F/g (23 F/cm(3))for the activated carbon (carbonized at 600 degrees C), comparable to 44 F/g (22 F/cm(3)) of commercial activated carbon (MSP). The corresponding values for the activated carbons (carbonized at 800 degrees C and 1000 degrees C) were 40 F/g (23 F/cm(3)) and 17 F/g (12 F/cm(3)), respectively. (C) 2017 Elsevier Ltd. All rights reserved.
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收藏
页码:1801 / 1808
页数:8
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