1,2-Dihydroxy-2-(3-methylbut-2-enyl)-3-oxo-2,3-dihydro-1H-indene-1-carboxylic acid monohydrate

被引：8
|
作者：
Franscisco, Acacio Ivo [2 ]
Silveira, Gleiciani de Q. [2 ]
Resende, Jackson A. L. C. [2 ]
Balliano, Tatiane L. [1 ]
Malta, Valeria R. S. [1 ]
Pinto, Antonio Ventura [3 ]
机构：
[1] Univ Fed Alagoas, Inst Quim & Biotecnol, BR-57072970 Maceio, Al, Brazil
[2] Univ Fed Fluminense, Inst Quim, BR-24020150 Niteroi, RJ, Brazil
[3] Univ Fed Rio de Janeiro, Nucleo Pesquisas Prod Nat, BR-21944971 Rio De Janeiro, Brazil
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷
关键词：
POTASSIUM-PERMANGANATE; HOOKER OXIDATION; DERIVATIVES; MECHANISM;
D O I：
10.1107/S1600536810000516
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title compound, C(15)H(16)O(5)center dot H(2)O, is an intermediate of the Hooker oxidation reaction, used for the synthesis of 2-hydroxy-3-(2-methylprop-1-enyl)naphthalene-1,4-dione (norlapachol). The packing in the crystal structure is arranged by an O-H center dot center dot center dot O hydrogen-bonded network along the [100] and [010] directions. Each organic molecule is linked to four other molecules via the hydroxy groups. The water solvent molecule is connected to carboxylic acid groups by three hydrogen bonds.
引用
收藏
页码：O341 / U2279
页数：10
相关论文
共 50 条
  • [21] 1-(Dicyanomethylene)-3-hydroxy-1H-indene-2-carboxylic Acid
    Usova, Sofia D.
    Knyazeva, Ekaterina A.
    Rakitin, Oleg A.
    MOLBANK, 2024, 2024 (03)
  • [22] SYNTHESIS AND ANTI-INFLAMMATORY ACTIVITIES OF SOME 2,3-DIHYDRO-1H-BENZ(E)INDENE-1-CARBOXYLIC AND 2,3-DIHYDRO-1H-BENZ(E)INDENE-CARBOXYLIC ACIDS
    ROVERI, P
    CAVRINI, V
    GATTI, R
    CESARONI, MR
    PAPPALARDO, MS
    CANDELETTI, S
    ARCHIV DER PHARMAZIE, 1983, 316 (04) : 309 - 315
  • [23] SYNTHESIS AND BIOLOGICAL EVALUATION OF ETHYL 2-[(3-METHYL-2-OXOQUINOXALIN-1(2H)-YL) ACETYL]-3-OXO-2,3-DIHYDRO-1H-PYRAZOLES
    Kotnal, Ramaling B.
    Rao, Gopal Krishna
    Pai, P. N. Sanjay
    INDIAN JOURNAL OF HETEROCYCLIC CHEMISTRY, 2011, 21 (01) : 45 - 48
  • [24] Trypanocidal activity of 1,3,7-trihydroxy-2-(3-methylbut-2-enyl)-xanthone isolated from Kielmeyera coriacea
    Caleare, Angelo de Oliveira
    Lazarin-Bidoia, Danielle
    Garcia Cortez, Diogenes A.
    Ueda-Nakamura, Tania
    Dias Filho, Benedito P.
    Silva, Sueli de Oliveira
    Nakamura, Celso Vataru
    PARASITOLOGY INTERNATIONAL, 2013, 62 (05) : 405 - 411
  • [25] Synthesis of oxazolo[3,2-a]quinolinium triiodide from 4-methyl-1-(3-methylbut-2-enyl)quinolin-2(1H)-one
    Vershinina, E. A.
    Kim, D. G.
    Slepukhin, P. A.
    CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2012, 47 (12) : 1596 - 1597
  • [26] Synthesis of oxazolo[3,2-a]quinolinium triiodide from 4-methyl-1-(3-methylbut-2-enyl)quinolin-2(1H)-one
    E. A. Vershinina
    D. G. Kim
    P. A. Slepukhin
    Chemistry of Heterocyclic Compounds, 2012, 47 : 1596 - 1597
  • [27] N,N′-Bis(3-methylbut-2-enyl)-N,N′-(1,4phenylene)dibenzenesulfonamide
    Ejaz
    Khan, Islam Ullah
    Sheikh, Tahir Ali
    Harrison, William T. A.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O3281 - U762
  • [28] 4,8-Dihydroxy-2,3-dimethoxy-1-(3methylbut-2-enyl)-9H-xanthen-9-one
    Boonnak, Nawong
    Chantrapromma, Suchada
    Fun, Hoong-Kun
    Karalai, Chatchanok
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O4903 - U6903
  • [29] 1-Acetyl-3-(2-chloro-2,3-dihydrobenzofuran-3-yl)-1,2-dihydro-3-hydroxy-2-oxo-3H-indole
    Usman, A
    Razak, IA
    Fun, HK
    Chantrapromma, S
    Zhang, Y
    Xu, JH
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2002, 58 : O37 - O39
  • [30] Unprecedented sigmatropic rearrangements leading to 2,3-dihydro-1H-2-benzazepine-3-carboxylic acid
    Martins, JC
    Van Rompaey, K
    Wittmann, G
    Tömböly, C
    Tóth, G
    De Kimpe, N
    Tourwé, D
    JOURNAL OF ORGANIC CHEMISTRY, 2001, 66 (08): : 2884 - 2886
12345