Two-dimensional Mossbauer spectrometer based on Arduino technology

被引:3
|
作者
Jahns, Moritz [1 ]
Pawlak, Justus [1 ]
Klimke, Stephen [1 ]
Sindelar, Ralf [2 ]
Schrewe, Ulrich [2 ]
Patzke, Robert [3 ]
Renz, Franz [1 ]
机构
[1] Leibniz Univ Hannover, Inst Anorgan Chem, Hannover, Germany
[2] Hsch Hannover, Fak Maschinenbau & Bioverfahrenstech 2, Hannover, Germany
[3] Hsch Hannover, Fak Elektro & Informat Tech 1, Hannover, Germany
关键词
Mossbauer spectroscopy; Two dimensional data acquisition; Peak height analysis; Arduino; CONVERSION X-RAY; ELECTRON;
D O I
10.1016/j.nima.2022.166529
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
Mossbauer (MB) spectroscopy is the most sensitive method for analysing iron compounds and complexes available. It is widely used to determine the spin state of switching iron complexes. A well-tuned Spectrometer is capable of obtaining spectra with proper signal to noise ratios. Therefore, selecting the correct energy range out of the whole spectrum of the Mossbauer source is crucial, especially, when complex samples are measured. In this paper, we show further development of our previous works - A functional two-dimensional Mossbauer spectrometer. The key part of our system is a two-dimensional counter array, which stores every photon event detected according to its energy and velocity. This enables us to calculate Mossbauer spectra in different energy ranges to tune a proper signal to noise ratio. For that, we show the drop of the signal to noise ratio when energy ranges are changed. Furthermore, as our approach handles every photon event detected, our system is capable of overserving not only one transition line. For Fe-57 there is, beside the 14.4 keV line, an X-ray emission at 6.4 keV from the internal conversion of absorbed gamma rays. With our approach it is possible to observe both lines simultaneously.
引用
收藏
页数:5
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